{Pt2(P(C2H5)3)2Cl4} in benzene isomerization; equilibrium;;
参考文献
Cahours, A.; Gal, H.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1870 , vol. 70, p. 902 - 902
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Cahours, A.; Gal, H.
Liebigs Annalen der Chemie, 1870 , vol. 155, p. 228 - 228
in toluene byproducts: CO; N2-atmosphere; filtration, drying (vac.);
参考文献
Abram, Ulrich; Belli Dell'Amico, Daniela; Calderazzo, Fausto; Marchetti, Lorella; Straehle, Joachim
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1999 , p. 4093 - 4098
in isopropyl alcohol; benzene soln. of Pt complex in benzene reacted with PEt3 soln. in i-PrOH, stirred for 2 h in N2 atm.; evapd., filtered, washed with pentane and crystd. in 95percent EtOH;
参考文献
Olgemoeller, Bernhard; Olgemoeller, Luitgard; Beck, Wolfgang
Chemische Berichte, 1981 , vol. 114, # 9 p. 2971 - 2978
in water shaking of a soln. of K2(PtCl4) in H2O with P(C2H5)3 for 1/2 h; heating of the ppt. in the mother-lye for 10 min at 100°C;; washing of the ppt. with H2O; extraction with ether; recrystallization in alcohol under addn. of active carbon;;
参考文献
Jensen, K. A.
Z. Anorg. Chem., 1936 , vol. 229, p. 225 - 251
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Gmelin Handbook: Pt: MVol.D, 157, page 346 - 348
