1,11-二(甲烷磺酰基氧基)-3,6,9-三氧杂十一烷合成路线 （共 18 条）
反应条件
Yield given. Multistep reaction;
参考文献
Talma, Auke G.; Vossen, Huib van; Sudhoelter, Ernst J. R.; Eerden, Johan van; Reinhoudt, David N.
Synthesis, 1986 , # 8 p. 680 - 683
反应条件
triethylamine in dichloromethane
T=20°C; 24 h;
参考文献
Bakleh; Sol; Estieu-Gionnet; Granet; Deleris; Krausz
Tetrahedron, 2009 , vol. 65, # 36 p. 7385 - 7392
反应条件
silver(l) oxide in dichloromethane
48 h;
参考文献
Svedhem; Hollander; Shi; Konradsson; Liedberg; Svensson
Journal of Organic Chemistry, 2001 , vol. 66, # 13 p. 4494 - 4503
反应条件
silver(l) oxide in dichloromethane
Inert atmosphere;
参考文献
Jalisatgi, Satish S.; Kulkarni, Vikas S.; Tang, Betty; Houston, Zachary H.; Lee, Mark W.; Hawthorne, M. Frederick
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12382 - 12385
反应条件
sodium iodide in acetone
Reflux;
参考文献
Jensen, Marie; Schmidt, Steffen; Fedosova, Natalya U.; Mollenhauer, Jan; Jensen, Henrik H.
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 7 p. 2407 - 2417
反应条件
1: sodium azide / N,N-dimethyl-formamide / 110 °C / Inert atmosphere
2: hydrogenchloride; triphenylphosphine / diethyl ether / Inert atmosphere
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 6 h / 0 °C / Inert atmosphere
4: triphenylphosphine / tetrahydrofuran; water / 24 h / 20 °C / Inert atmosphere
5: silver(l) oxide / dichloromethane / Inert atmosphere
View Scheme
参考文献
Jalisatgi, Satish S.; Kulkarni, Vikas S.; Tang, Betty; Houston, Zachary H.; Lee, Mark W.; Hawthorne, M. Frederick
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12382 - 12385
反应条件
(i) Na, (ii) /BRN= 1890100/; Multistep reaction;
参考文献
Newman,M.S. et al.
Journal of Organic Chemistry, 1975 , vol. 40, p. 2863 - 2870
反应条件
2: 80 percent / polyphosphoric acid / acetic acid / 60 °C
3: 91 percent / sodium borohydride / ethanol / 18 h / Ambient temperature
4: 90 percent / pyridinium tosylate / benzene / 18 h / Heating
View Scheme
参考文献
Talma, Auke G.; Vossen, Huib van; Sudhoelter, Ernst J. R.; Eerden, Johan van; Reinhoudt, David N.
Synthesis, 1986 , # 8 p. 680 - 683
