反应条件
1.1: NaH / hexane; 1,2-dimethoxy-ethane / 0.5 h / 0 °C
1.2: 65 percent / hexane; 1,2-dimethoxy-ethane / 19 h / 0 - 20 °C
2.1: 52 percent / N2H4*H2O; NaOH / triethylene glycol / 7 h / Heating
View Scheme
参考文献
Chavan, Subhash P.; Kharul, Rajendra K.; Kale, Ramesh R.; Khobragade, Dushant A.
Tetrahedron, 2003 , vol. 59, # 15 p. 2737 - 2741
