(Z)-3-己烯醛二甲基缩醛合成路线 （共 10 条）
反应条件
oxalic acid; benzene-1,2-diol in water; acetone T=45 - 50°C;
参考文献
Winter,M.
Helvetica Chimica Acta, 1963 , vol. 46, p. 1792 - 1797
反应条件
K-O-Bu-t in tetrahydrofuran
T=-10 - 20°C; Wittig reaction;
参考文献
Li, Hao; Loh, Teck-Peng
Journal of the American Chemical Society, 2008 , vol. 130, # 23 p. 7194 - 7195
反应条件
1: 58 percent / 18 h / 100 °C
2: HCO2H, Et3N / 10percent Pd/C / 18 h / 100 °C
View Scheme
参考文献
Weir, John R.; Patel, Babu A.; Heck, Richard F.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4926 - 4931
反应条件
formic acid; triethylamine; palladium on activated charcoal
T=100°C; 18 h;
参考文献
Weir, John R.; Patel, Babu A.; Heck, Richard F.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4926 - 4931
反应条件
formic acid; triethylamine; palladium on activated charcoal
T=100°C; 18 h;
参考文献
Weir, John R.; Patel, Babu A.; Heck, Richard F.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4926 - 4931
反应条件
formic acid; triethylamine; palladium on activated charcoal
T=100°C; 13 h;
参考文献
Weir, John R.; Patel, Babu A.; Heck, Richard F.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4926 - 4931
反应条件
1: 61 percent / diethyl ether / 18 h / Ambient temperature
2: HCO2H, Et3N / 10percent Pd/C / 13 h / 100 °C
View Scheme
参考文献
Weir, John R.; Patel, Babu A.; Heck, Richard F.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4926 - 4931
反应条件
hydrogen; Lindlar's catalyst in hexane
参考文献
Winter,M.
Helvetica Chimica Acta, 1963 , vol. 46, p. 1792 - 1797
反应条件
1: NaOMe / 24 h / 110 - 115 °C
2: H2 / Lindlar catalyst / hexane
View Scheme
参考文献
Winter,M.
Helvetica Chimica Acta, 1963 , vol. 46, p. 1792 - 1797
反应条件
CH3C6H4SO3H
4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kulinkovich, O. G.; Tishchenko, I. G.; Sorokin, V. L.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 8 p. 1519 - 1525
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 8 p. 1663 - 1670
