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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
55459-60-4
合成路线
（共 10 条）
55459-60-4
→
反应条件
87642-29-3
3-苯基-4,5,6,7-四氢-1H-吡唑并[4,3-c]吡啶
反应条件
1: triethylamine / CH2Cl2 / 20 h / Ambient temperature 2: 98percent hydrazine hydrate / aq. ethanol / 3 h / Ambient temperature 3: 78 percent / 10percent aq.HCl / 2 h / Heating View Scheme
参考文献
Winters, Giorgio; Sala, Alberto; Barone, Domenico; Baldoli, Emiliana
Journal of Medicinal Chemistry, 1985 , vol. 28, # 7 p. 934 - 940
110-91-8
吗啉
+
32161-06-1
N-乙酰基-4-哌啶酮
→
反应条件
55459-60-4
反应条件
titanium tetrachloride in benzene T=50°C; 1 h;
参考文献
Nilsson, Asa; Carlson, Rolf
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 6 p. 523 - 525
55459-60-4
→
反应条件
87628-26-0
反应条件
1: triethylamine / CH2Cl2 / 20 h / Ambient temperature 2: 98percent hydrazine hydrate / aq. ethanol / 3 h / Ambient temperature View Scheme
参考文献
Winters, Giorgio; Sala, Alberto; Barone, Domenico; Baldoli, Emiliana
Journal of Medicinal Chemistry, 1985 , vol. 28, # 7 p. 934 - 940
55459-60-4
→
反应条件
87628-42-0
3-(4-甲氧基苯基)-4,5,6,7-四氢-1H-吡唑并[4,3-c]吡啶
反应条件
1: triethylamine / CH2Cl2 / 20 h / Ambient temperature 2: 98percent hydrazine hydrate / aq. ethanol / 3 h / Ambient temperature 3: 85 percent / 10percent aq.HCl / 2 h / Heating View Scheme
参考文献
Winters, Giorgio; Sala, Alberto; Barone, Domenico; Baldoli, Emiliana
Journal of Medicinal Chemistry, 1985 , vol. 28, # 7 p. 934 - 940
55459-60-4
→
反应条件
87628-44-2
反应条件
1: triethylamine / CH2Cl2 / 20 h / Ambient temperature 2: 98percent hydrazine hydrate / aq. ethanol / 3 h / Ambient temperature 3: 80 percent / 10percent aq.HCl / 2 h / Heating View Scheme
参考文献
Winters, Giorgio; Sala, Alberto; Barone, Domenico; Baldoli, Emiliana
Journal of Medicinal Chemistry, 1985 , vol. 28, # 7 p. 934 - 940
55459-60-4
→
反应条件
87628-46-4
反应条件
1: triethylamine / CH2Cl2 / 20 h / Ambient temperature 2: 98percent hydrazine hydrate / aq. ethanol / 3 h / Ambient temperature 3: 70 percent / 10percent aq.HCl / 2 h / Heating View Scheme
参考文献
Winters, Giorgio; Sala, Alberto; Barone, Domenico; Baldoli, Emiliana
Journal of Medicinal Chemistry, 1985 , vol. 28, # 7 p. 934 - 940
55459-60-4
→
反应条件
87628-48-6
反应条件
1: triethylamine / CH2Cl2 / 20 h / Ambient temperature 2: 98percent hydrazine hydrate / aq. ethanol / 3 h / Ambient temperature 3: 93 percent / 10percent aq.HCl / 2 h / Heating View Scheme
参考文献
Winters, Giorgio; Sala, Alberto; Barone, Domenico; Baldoli, Emiliana
Journal of Medicinal Chemistry, 1985 , vol. 28, # 7 p. 934 - 940
403-43-0
对氟苯甲酰氯
+
55459-60-4
→
反应条件
87642-26-0
反应条件
triethylamine in dichloromethane 20 h; Ambient temperature;
参考文献
Winters, Giorgio; Sala, Alberto; Barone, Domenico; Baldoli, Emiliana
Journal of Medicinal Chemistry, 1985 , vol. 28, # 7 p. 934 - 940
55459-60-4
→
反应条件
87642-26-0
反应条件
1: Et3N / CH2Cl2 / 0 - 20 °C 2: 5percent HCl / CH2Cl2 / 0.5 h / Ambient temperature View Scheme
参考文献
Sanfilippo, PJ; Urbanski, M; Williams, L; Press, JB; Katz, LB; et al.
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 7 p. 655 - 661
55459-60-4
→
反应条件
87642-32-8
反应条件
1: triethylamine / CH2Cl2 / 20 h / Ambient temperature 2: 98percent hydrazine hydrate / aq. ethanol / 3 h / Ambient temperature 3: 64 percent / 10percent aq.HCl / 2 h / Heating View Scheme
参考文献
Winters, Giorgio; Sala, Alberto; Barone, Domenico; Baldoli, Emiliana
Journal of Medicinal Chemistry, 1985 , vol. 28, # 7 p. 934 - 940
