2-叔丁氧羰基氨基丙烯酸甲酯合成路线 (共 79 条)
反应条件
1: m-CPBA 2: toluene / 110 °C View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 180, # 5-6 p. 1203 - 1208
反应条件
potassium carbonate in methanol 2 h;
参考文献
Tedaldi, Lauren M.; Smith, Mark E. B.; Nathani, Ramiz I.; Baker, James R.
Chemical Communications, 2009 , # 43 p. 6583 - 6585
反应条件
potassium carbonate in methanol 0.166667 h;
参考文献
Tedaldi, Lauren M.; Smith, Mark E. B.; Nathani, Ramiz I.; Baker, James R.
Chemical Communications, 2009 , # 43 p. 6583 - 6585
反应条件
caesium carbonate in methanol 4 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 28, # 36 p. 4185 - 4188
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene Heating;
参考文献
Goodall, Karen; Parsons, Andrew F.
Tetrahedron Letters, 1995 , vol. 36, # 18 p. 3259 - 3260
反应条件
1.1: lithium selenolate / diethyl ether / 0 °C 1.2: 49 percent / diethyl ether / 20 h / 20 °C 2.1: H2O2 View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 3, # 13 p. 2476 - 2481
反应条件
1: 95 percent / MeOH / benzene 2: 85 percent / PPh3; DEAD / toluene / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 12, # 21 p. 3129 - 3133
反应条件
1: NaOMe / methanol 2: triethylbenzylammonium chloride, KOH 3: 1. NaH 2. NaI / 1. dimethoxyethane, -10 deg C -> room temp. View Scheme
参考文献
Journal of Organic Chemistry, , vol. 55, # 13 p. 3998 - 4006
反应条件
in diethyl ether T=-60°C; 3 h; Yield given. Title compound not separated from byproducts;
参考文献
Bajgrowicz, J. A.; Hallaoui, A. El; Jacquier, R.; Pigiere, Ch.; Viallefont, Ph.
Tetrahedron Letters, 1984 , vol. 25, # 26 p. 2759 - 2762
反应条件
in diethyl ether T=-60°C; 3 h; Yield given. Title compound not separated from byproducts;
参考文献
Bajgrowicz, J. A.; Hallaoui, A. El; Jacquier, R.; Pigiere, Ch.; Viallefont, Ph.
Tetrahedron, 1985 , vol. 41, # 10 p. 1833 - 1845