2-叔丁氧羰基氨基丙烯酸甲酯合成路线 （共 79 条）
反应条件
copper(l) iodide; di-n-butyl sulfide 1.) Et2O, -60 deg C, 30 min; 2.) Et2O, -60 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 41, # 10 p. 1833 - 1845
反应条件
copper(l) iodide; di-n-butyl sulfide 1.) Et2O, -60 deg C, 30 min; 2.) Et2O, -60 deg C, 18 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 41, # 10 p. 1833 - 1845
反应条件
copper(l) iodide 1.) Et2O, -60 deg C, 30 min; 2.) Et2O, -10 deg C, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 41, # 10 p. 1833 - 1845
反应条件
copper(l) iodide 1.) Et2O, -60 deg C, 30 min; 2.) Et2O, -60 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 41, # 10 p. 1833 - 1845
反应条件
copper(l) iodide 1.) Et2O, -60 deg C, 30 min; 2.) Et2O, -60 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 41, # 10 p. 1833 - 1845
反应条件
copper(l) iodide 1.) Et2O, -60 deg C, 30 min; 2.) Et2O, -60 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 41, # 10 p. 1833 - 1845
反应条件
solid-phase synthesis; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 39, # 3-4 p. 289 - 292
反应条件
1: With tetrabutyl-ammonium chloride; sodium formate; sodium hydrogencarbonate; palladium diacetate; sodium chloride Heck coupling; 1 h; 2: With acetic anhydride 12 h; Heating;
参考文献
Tullberg, Erik; Schacher, Felix; Peters, Dan; Frejd, Torbjoern
Synthesis, 2006 , # 7 p. 1183 - 1189
反应条件
Rh(1+)*2CH4O*C4H12B(1-)*C34H40O2P2; hydrogen in methanol T=22°C; P=750.075 Torr; 0.0666667 h; Inert atmosphere; enantioselective reaction;
参考文献
Mohar, Barbara; Stephan, Michel
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 2-3 p. 594 - 600
反应条件
1: With (S)-difluoroPhos; tetrakis-(ethylene)-μ,μ'-dichlorodirhodium(I); sodium hydrogencarbonate 0.166667 h; Inert atmosphere; 2: in isopropyl alcohol T=25°C; 20 h; Inert atmosphere; enantioselective reaction;
参考文献
Diverchim; Darses, Sylvain; Lefevre, Nicolas; Folleas, Benoit; Brayer, Jean-Louis
Patent: US2014/12005 A1, 2014 ;
Location in patent: Paragraph 0399 - 0407 ;
