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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
55484-03-2
合成路线
（共 28 条）
110-00-9
呋喃
+
109-09-1
2-氯吡啶
→
反应条件
55484-03-2
反应条件
1: furan With n-butyllithium 2: With zinc(II) chloride 3: alpha-chloropyridine With nickel phosphine amido pincer complex in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=70°C; Negishi cross-coupling; 12 h; Further stages.;
参考文献
Wang, Li; Wang, Zhong-Xia
Organic Letters, 2007 , vol. 9, # 21 p. 4335 - 4338
24244-60-8
2-(苯磺酰基)吡啶
→
反应条件
55484-03-2
反应条件
1: 2-bromofuran With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.666667 h; 2: 2-benzenesulfonyl pyridine in tetrahydrofuran; hexane T=-78°C; 3.16667 h;
参考文献
Kuraray Co., Ltd.
Patent: EP1548005 A1, 2005 ;
Location in patent: Page/Page column 12-13 ;
110-00-9
呋喃
+
109-04-6
邻溴吡啶
→
反应条件
55484-03-2
反应条件
1: furan With (nBu)3MgLi in tetrahydrofuran T=20°C; 2 h; 2: 2-bromo-pyridine With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 18 h; Heating;
参考文献
Mongin, Florence; Bucher, Aurelien; Bazureau, Jean Pierre; Bayh, Omar; Awad, Hacan; Trecourt, Francois
Tetrahedron Letters, 2005 , vol. 46, # 46 p. 7989 - 7992
109-04-6
邻溴吡啶
+
13331-23-2
2-呋喃硼酸
→
反应条件
55484-03-2
反应条件
PdCl2(PPh3)2; potassium carbonate in ethylene glycol dimethyl ether; water T=80°C; 14 h;
参考文献
Pospech, Jola; Tlili, Anis; Spannenberg, Anke; Neumann, Helfried; Beller, Matthias
Chemistry - A European Journal, 2014 , vol. 20, # 11 p. 3135 - 3141
166328-14-9
2-呋喃三氟硼酸钾
+
109-09-1
2-氯吡啶
→
反应条件
55484-03-2
反应条件
palladium diacetate; sodium carbonate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in ethanol T=85°C; Suzuki-Miyaura coupling; 28 h; Inert atmosphere;
参考文献
Molander, Gary A.; Canturk, Belgin; Kennedy, Lauren E.
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 973 - 980
5029-67-4
2-碘吡啶
+
118486-94-5
2-(三丁基锡烷基)呋喃
→
反应条件
55484-03-2
反应条件
palladium 10 on activated carbon; LiF in 1-methyl-pyrrolidin-2-one T=120°C; Stille coupling; 24 h;
参考文献
Yabe, Yuki; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2010 , vol. 66, # 45 p. 8654 - 8660
85577-66-8
→
反应条件
55484-03-2
反应条件
copper T=160 - 220°C; P=12 Torr;
参考文献
Ribereau; Queguiner
Canadian Journal of Chemistry, 1983 , vol. 61, # 2 p. 334 - 342
33675-27-3
+
81745-86-0
→
反应条件
55484-03-2
反应条件
C32H26ClN2NiP in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=85°C; 12 h; Inert atmosphere;
参考文献
Zhang, Xue-Qi; Wang, Zhong-Xia
Journal of Organic Chemistry, 2012 , vol. 77, # 7 p. 3658 - 3663
109-09-1
2-氯吡啶
+
13331-23-2
2-呋喃硼酸
→
反应条件
55484-03-2
反应条件
potassium phosphate; C43H37ClFeNiP2*C4H8O in 1,4-dioxane T=70°C; Suzuki-Miyaura Coupling; 8 h; Inert atmosphere;
参考文献
Ge, Shaozhong; Hartwig, John F.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 51 p. 12837 - 12841
Angew. Chem.
372-48-5
2-氟吡啶
+
81745-86-0
→
反应条件
55484-03-2
反应条件
1: 2-fluoro-pyridine; (2-furyl)zinc chloride With Ni(PCy3)2Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=25 - 100°C; 10 h; Schlenk techniqueInert atmosphere; 2: (2-furyl)zinc chloride in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=100°C; 10 h; Inert atmosphereSchlenk technique;
参考文献
Zhu, Feng; Wang, Zhong-Xia
Journal of Organic Chemistry, 2014 , vol. 79, # 10 p. 4285 - 4292
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