4-氧基-苯氨基-2-巴豆酸合成路线 (共 14 条)
反应条件
sulfuric acid in dimethyl sulfoxide; toluene Cyclization; Heating;
参考文献
Miller, Christopher W.; Hoyle, Charles E.; Valente, Edward J.; Magers, David H.; Joensson, E. Sonny
Journal of Physical Chemistry A, 1999 , vol. 103, # 32 p. 6406 - 6412
反应条件
thionyl chloride; triethylamine in tetrahydrofuran T=20°C; 6.5 h; Reflux;
参考文献
Faturaci, Yeliz; Coskun, Necdet
Turkish Journal of Chemistry, 2012 , vol. 36, # 5 p. 749 - 758
反应条件
2,4,6-trichloro-1,3,5-triazine; triethylamine in dichloromethane T=20°C; 8 h;
参考文献
Haval, Kishan P.; Mhaske, Santosh B.; Argade, Narshinha P.
Tetrahedron, 2006 , vol. 62, # 5 p. 937 - 942
反应条件
1: 87 percent / thionyl chloride / CH2Cl2 / Heating 2: 85 percent / Et3N / diethyl ether / 2 h 3: 78 percent / Zn; acetic acid / 1 h / Heating View Scheme
参考文献
Pal, Bikash; Pradhan, Prasun K.; Jaisankar, Parasuraman; Giri, Venkatachalam S.
Synthesis, 2003 , # 10 p. 1549 - 1552
反应条件
in N,N-dimethyl-formamide 3 h; Heating;
参考文献
Balasubramaniyan, V.; Balasubramaniyan, P.; Shaikh, A. S.
Tetrahedron, 1986 , vol. 42, # 10 p. 2731 - 2738
反应条件
1: 51 percent / phosphorus pentoxide / 6 h / Heating 2: 63 percent / aniline / ethanol / 3 h / Heating 3: 75 percent / dimethylformamide / 5 h / Heating View Scheme
参考文献
Gupta; Wagh
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 3 p. 697 - 702
反应条件
thionyl chloride in dichloromethane Heating;
参考文献
Gaina, Constantin; Gaina, Viorica
Revue Roumaine de Chimie, 2005 , vol. 50, # 7-8 p. 655 - 661
反应条件
thionyl chloride; triethylamine in tetrahydrofuran T=20°C; 6.5 h; Reflux;
参考文献
Faturaci, Yeliz; Coskun, Necdet
Turkish Journal of Chemistry, 2012 , vol. 36, # 5 p. 749 - 758
反应条件
1: acetic anhydride; sodium acetate
2: ClSO3
View Scheme
参考文献
Correa; Cechinel Filho; Rosa; Isolani Pereira; Schlemper; Nunes
Pharmaceutical Sciences, 1997 , vol. 3, # 2 p. 67 - 71
参考文献
Patel, M. V.; Balasubramaniyan, V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. <B> 20, # 9 p. 804 - 805