3-甲基-2-(甲硫基)苯并噻唑鎓对甲苯磺酸盐合成路线 （共 8 条）
反应条件
in N,N-dimethyl-formamide
T=20 - 120°C;
参考文献
CANCER RESEARCH TECHNOLOGY LIMITED
Patent: US2009/247579 A1, 2009 ;
Location in patent: Page/Page column 35 ;
参考文献
PE Corporation (NY)
Patent: US6348596 B1, 2002 ;
反应条件
1: aqueous NaOH
View Scheme
参考文献
Beilenson; Hamer
Journal of the Chemical Society, 1939 , p. 143,149
反应条件
1: N,N-dimethyl-formamide / 4 h / 130 - 140 °C
2: triethylamine / ethanol / 1 h / 90 °C
3: 4 h / 125 °C
View Scheme
参考文献
Li, Xiaokai; Srinivasan, Sharan R.; Connarn, Jamie; Ahmad, Atta; Young, Zapporah T.; Kabza, Adam M.; Zuiderweg, Erik. R. P.; Sun, Duxin; Gestwicki, Jason E.
ACS Medicinal Chemistry Letters, 2013 , vol. 4, # 11 p. 1042 - 1047
参考文献
Fry; Kendall
Journal of the Chemical Society, 1951 , p. 1723,1725
反应条件
1: CH3I / 155 - 160 °C
View Scheme
参考文献
Fry; Kendall
Journal of the Chemical Society, 1951 , p. 1723,1725
反应条件
trimethylsilyl trifluoromethanesulfonate; triethylamine; lithium diisopropyl amide; trichlorophosphate; N-methyl-acetamide in methanol; dichloromethane; chloroform; ethyl acetate
参考文献
Molecular Probes, Inc.
Patent: US5436134 A1, 1995 ;
反应条件
triethylamine in ethanol
Heating;
参考文献
Van Allan,J.A. et al.
Journal of Heterocyclic Chemistry, 1975 , vol. 12, p. 1005 - 1007
