三甲基硅烷基 3-甲基丁酸酯合成路线 （共 5 条）
反应条件
p-trifluoromethylthiobenzoic anhydride; silver trifluoromethanesulfonate; titanium tetrachloride in dichloromethane 6 h; Ambient temperature;
参考文献
Miyashita, Mitsutomo; Shiina, Isamu; Miyoshi, So; Mukaiyama, Teruaki
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 5 p. 1516 - 1527
反应条件
sodium hydride in tetrahydrofuran
参考文献
Kuwajima,I. et al.
Tetrahedron Letters, 1976 , p. 1591 - 1594
反应条件
in acetonitrile
T=20°C; 0.25 h; Inert atmosphere;
参考文献
Zambron, Bartosz K.; Dubbaka, Srinivas R.; Markovic, Dean; Moreno-Clavijo, Elena; Vogel, Pierre
Organic Letters, 2013 , vol. 15, # 10 p. 2550 - 2553
反应条件
1: (-)-atractyloside potassium salt 2 h; HeatingAcidic conditions;
2: N-(trimethylsilyl)-imidazole With pyridine
T=100°C; 2 h; Inert atmosphere;
参考文献
Chen, Liang-Yu; Hu, Anren; Chang, Chih-Jui
Molecules, 2013 , vol. 18, # 2 p. 2018 - 2028
反应条件
tin(II) trifluoromethanesulfonate; p-trifluoromethylthiobenzoic anhydride in dichloromethane
3 h; Ambient temperature;
参考文献
Mukaiyama, Teruaki; Shiina, Isamu; Miyashita, Mitsutomo
Chemistry Letters, 1992 , # 4 p. 625 - 628
