1-环丙基-1-苯基乙醇合成路线 （共 19 条）
反应条件
lithium dimethyl cuprate in diethyl ether T=0°C; 1 h; or (CH3)2CuLi*LiBr; variations of times, solvent; MechanismProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 49, # 10 p. 1739 - 1743
参考文献
Journal of Organic Chemistry, , vol. 70, # 17 p. 6820 - 6826
反应条件
1: AlCl3 / 35 - 60 °C 2: diethyl ether View Scheme
参考文献
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 43, p. 1164
Chem. Zentralbl., , vol. 83, # I p. 1458
反应条件
lithium aluminium tetrahydride; alpha,alpha-dimethylbenzyl hydroperoxide; oxygen 1) cumene, heating; Yield givenMultistep reaction;
参考文献
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), , vol. 341, # 1 p. 52 - 58
反应条件
(i) aq. Hg(OAc)2, THF, (ii) NaBH4, aq. NaOH; Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 156, p. 37 - 44
参考文献
Journal of Organometallic Chemistry, , vol. 156, p. 37 - 44
反应条件
hydrogen bromide; lithium bromide in water T=0°C; 2 h; Inert atmosphere;
参考文献
Singh, Fateh V.; Wirth, Thomas
Organic Letters, 2011 , vol. 13, # 24 p. 6504 - 6507
反应条件
[bis(acetoxy)iodo]benzene; iodine in dichloromethane T=20°C; 0.25 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 70, # 17 p. 6820 - 6826
反应条件
1.1: sodium hydride / tetrahydrofuran / 0.75 h / 0 - 20 °C / |Inert atmosphere
1.2: 24 h / 20 °C / |Inert atmosphere
2.1: N,N,N',N'-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a;2',1'-c][1,4] diazepine-2,12-diamine / N,N-dimethyl-formamide / 72 h / |Inert atmosphere; |Glovebox; |UV-irradiation
View Scheme
参考文献
Doni, Eswararao; O'Sullivan, Steven; Murphy, John A.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 8 p. 2239 - 2242
Angew. Chem., 2013 , vol. 125, # 8 p. 2295 - 2298,4
