反应条件
1: lithium aluminium tetrahydride / diethyl ether / 3.5 h / 20 °C / Inert atmosphere; Reflux
2: [Ca((2,6-diisopropylphenyl)NC(CH3)CHC(CH3)N(2,6-diisopropylphenyl))(N(SiMe3)2)(THF)] / benzene / 0.25 h / 25 °C / Inert atmosphere
View Scheme
参考文献
Crimmin, Mark R.; Arrowsmith, Merle; Barrett, Anthony G. M.; Casely, Ian J.; Hill, Michael S.; Procopiou, Panayiotis A.
Journal of the American Chemical Society, 2009 , vol. 131, # 28 p. 9670 - 9685
