sodium hydroxide in methanol 8 h; Heating;

diisobutylaluminium hydride in diethyl ether

1.1: LiAlH4 / diethyl ether / Heating 1.2: 60 percent / H2O; NaOH / diethyl ether / 2 h / 20 °C 2.1: 95 percent Spectr. / 1,3-bis(2-iPrC6H4)-2-bis(TMS)N-2,1,3-scandiadiazolidine / benzene / 72 h / 120 °C View Scheme

3-chloro-benzenecarboperoxoic acid in chloroform T=20°C; 16 h;