4-二乙基氨基-2-甲氧基-苯甲醛合成路线 （共 3 条）
反应条件
1: 4-(diethylamino)-2-hydroxybenzaldehyde With potassium hydroxide; potassium carbonate in acetonitrile T=80°C; 0.166667 h; 2: methyl iodide in acetonitrile T=80°C; 2 h; Further stages.;
参考文献
Chou, Pi-Tai; Huang, Chien-Huang; Pu, Shih-Chieh; Cheng, Yi-Ming; Liu, Yi-Hong; Wang, Yu; Chen, Chao-Tsen
Journal of Physical Chemistry A, 2004 , vol. 108, # 31 p. 6452 - 6454
反应条件
potassium carbonate in N,N-dimethyl-formamide T=50°C; 8 h;
参考文献
Kim, Byung-Soon; Kashibuchi, Daisuke; Son, Young-A.; Kim, Sung-Hoon; Matsumoto, Shinya
Dyes and Pigments, 2011 , vol. 90, # 1 p. 56 - 64
反应条件
1: 90 percent / tetrahydrofuran / 1 h / 20 °C
2: 64 percent / DDQ / dioxane / 4 h / 20 °C
3: 58 percent / BBr3 / CH2Cl2 / -78 - 20 °C
View Scheme
参考文献
Chou, Pi-Tai; Huang, Chien-Huang; Pu, Shih-Chieh; Cheng, Yi-Ming; Liu, Yi-Hong; Wang, Yu; Chen, Chao-Tsen
Journal of Physical Chemistry A, 2004 , vol. 108, # 31 p. 6452 - 6454
