1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯合成路线 （共 21 条）
55591-23-61,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
→
反应条件
dichlorotris(triphenylphosphine)ruthenium(II) in pentane T=120°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Kamigata, Nobumasa; Ohtsuka, Takeshi; Fukushima, Takamasa; Yoshida, Masato; Shimizu, Toshio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 10 p. 1339 - 1346
55591-23-61,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯+
→
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene T=120°C; 7 h;
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 129, p. 155 - 168
55591-23-61,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
→
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene T=120°C; 7 h;
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 129, p. 155 - 168
55591-23-61,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
→
反应条件
dichlorotris(triphenylphosphine)ruthenium(II) in pentane T=120°C; 24 h;
参考文献
Kamigata, Nobumasa; Ohtsuka, Takeshi; Shimizu, Toshio
Phosphorus, Sulfur and Silicon and the Related Elements, 1994 , vol. 96, # 1-4 p. 491 - 492
→
55591-23-61,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
反应条件
in N,N-dimethyl-formamide
in presence of Co powder, 20-60°C;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
→
55591-23-61,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
反应条件
zinc in water; dimethyl sulfoxide
80°C, chlorination at 35°C;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
→
55591-23-61,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
反应条件
in hydrogenchloride
oxidn., in a 5 percent HCl soln.,;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
→
55591-23-61,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
反应条件
Zn and Cu in dimethyl sulfoxide
suspension of Zn and Cu in (CH3)2SO;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
55591-23-61,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
→
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene
T=120°C; 18 h;
参考文献
Kamigata, Nobumasa; Fukushima, Takamasa; Terakawa, Yoshie; Yoshida, Masato; Sawada, Hideo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 3 p. 627 - 633
55591-23-61,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
→
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene
T=120°C; 18 h;
参考文献
Kamigata, Nobumasa; Fukushima, Takamasa; Terakawa, Yoshie; Yoshida, Masato; Sawada, Hideo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 3 p. 627 - 633
