1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯 合成路线 （共 21 条）
55591-23-6 1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
→
反应条件
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene
T=120°C; 18 h;
参考文献
Kamigata, Nobumasa; Fukushima, Takamasa; Terakawa, Yoshie; Yoshida, Masato; Sawada, Hideo
55591-23-6 1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
→
反应条件
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene
T=120°C; 18 h;
参考文献
Kamigata, Nobumasa; Fukushima, Takamasa; Terakawa, Yoshie; Yoshida, Masato; Sawada, Hideo
55591-23-6 1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
→
反应条件
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene
T=120°C; 18 h;
参考文献
Kamigata, Nobumasa; Fukushima, Takamasa; Terakawa, Yoshie; Yoshida, Masato; Sawada, Hideo
55591-23-6 1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
→
反应条件
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene
T=120°C; 18 h;
参考文献
Kamigata, Nobumasa; Fukushima, Takamasa; Terakawa, Yoshie; Yoshida, Masato; Sawada, Hideo
55591-23-6 1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
→
反应条件
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene
T=120°C; 18 h;
参考文献
Kamigata, Nobumasa; Fukushima, Takamasa; Terakawa, Yoshie; Yoshida, Masato; Sawada, Hideo
55591-23-6 1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
→
反应条件
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene
T=120°C; 18 h;
参考文献
Kamigata, Nobumasa; Fukushima, Takamasa; Terakawa, Yoshie; Yoshida, Masato; Sawada, Hideo
55591-23-6 1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯 +
→
反应条件
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene
T=120°C; 18 h;
参考文献
Kamigata, Nobumasa; Fukushima, Takamasa; Terakawa, Yoshie; Yoshida, Masato; Sawada, Hideo
55591-23-6 1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯 +
→
反应条件
反应条件
dichlorotris(triphenylphosphine)ruthenium(II) in pentane
T=120°C; 19 h; further aromatic and heteroaromatic compounds; Product distributionMechanism;
参考文献
Kamigata, Nobumasa; Ohtsuka, Takeshi; Fukushima, Takamasa; Yoshida, Masato; Shimizu, Toshio
55591-23-6 1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
→
反应条件
反应条件
ammonia in tetrachloromethane
参考文献
Podol'skii, A. V.; Kachalkova, M. I.; Ilatovskii, R. E.; Kodess, M. I.; Kolenko, I. P.
55591-23-6 1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯 +
→
反应条件
反应条件
in diethyl ether; water
to a soln. of ((C2H5)4N)N3 in ether containing 1 percent H2O was added C6F13SO2Cl at 0°C, vigorous stiriring, then stirring at 20°C, 20 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.3, page 137 - 151
