water in water; toluene; butan-1-ol (CH3)2SiCl2 and (CH3)SiCl3 (1:1 mol) in butanol-H2O-toluene; heating of the oily product at 350-600°C in a slow stream of N2;; distn.; crystn. on cooling; recrystn. from toluene;;
参考文献
Journal of the American Chemical Society, , vol. 68, p. 356 - 358