Voronkov, M. G.; Tsyrendorzhieva, I. P.; Albanov, A. I.; Shergina, N. I.; Klyba, L. V.; Dubinskaya, E. I.
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 654 - 655
Zhurnal Obshchei Khimii, 1998 , vol. 68, # 4 p. 695 - 696
CoCl2 in acetonitrile 168 h; Ambient temperatureother acyl chlorides; also in the presence of hexamethyldisiloxane or trimethylacetoxysilane; Product distribution;
参考文献
Basenko, S. V.; Ogorodnikova, E. I.; Vitkovskii, V. Yu.; Mirskov, R. G.; Voronkov, M. G.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 1.1 p. 97 - 102,79 - 83
sulfuric acid; antimony pentachloride in tetrachloromethane; sulfuric acid shaking of (CH3)3SiOSi(CH3)3 and ((CH3)2SiO)4 (1:1 mol) with concd. H2SO4 at 25°C for 8 days; equilibrium react.; further products;;
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Gen.Electric Co.
Patent: US2469890 , 1946 ;
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Patnode; Wilcock
Journal of the American Chemical Society, 1946 , vol. 68, p. 360,363
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Scott
Journal of the American Chemical Society, 1946 , vol. 68, p. 2295
H2SO4 in sulfuric acid aq. H2SO4; shaking of (CH3)3SiOSi(CH3)3 and ((CH3)2SiO)4 with concd. H2SO4 at room temp. for 4 h;;
参考文献
Patnode, W. I.; Wilcock, D. F.
Journal of the American Chemical Society, 1946 , vol. 68, p. 358 - 363
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Gmelin Handbook: Si: MVol.C, 103, page 282 - 285
T=190°C; 10 h; Yield givenFurther byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Voronkov, M. G.; Tsyrendorzhieva, I. P.; Albanov, A. I.; Shergina, N. I.; Klyba, L. V.; Dubinskaya, E. I.
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 654 - 655
Zhurnal Obshchei Khimii, 1998 , vol. 68, # 4 p. 695 - 696
