sulfuric acid; antimony pentachloride in tetrachloromethane; sulfuric acid shaking of (CH3)3SiOSi(CH3)3 and ((CH3)2SiO)4 (1:1 mol) with concd. H2SO4 at 25°C for 8 days; equilibrium react.; further products;;
sulfuric acid; antimony pentachloride in tetrachloromethane; sulfuric acid shaking of (CH3)3SiOSi(CH3)3 and ((CH3)2SiO)4 (1:1 mol) with concd. H2SO4 at 25°C for 8 days; equilibrium react.; further products;;
H2SO4 in sulfuric acid aq. H2SO4; shaking of (CH3)3SiOSi(CH3)3 and ((CH3)2SiO)4 with concd. H2SO4 at room temp. for 4 h;;
参考文献
Patnode, W. I.; Wilcock, D. F.
Journal of the American Chemical Society, 1946 , vol. 68, p. 358 - 363
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Gmelin Handbook: Si: MVol.C, 103, page 282 - 285
T=190°C; 10 h; Yield givenFurther byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Voronkov, M. G.; Tsyrendorzhieva, I. P.; Albanov, A. I.; Shergina, N. I.; Klyba, L. V.; Dubinskaya, E. I.
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 654 - 655
Zhurnal Obshchei Khimii, 1998 , vol. 68, # 4 p. 695 - 696
