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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
异戊烯醇
合成路线
（共 369 条）
100-66-3
苯甲醚
+
556-82-1
异戊烯醇
→
反应条件
4957-18-0
+
4957-17-9
+
18491-21-9
+
18272-85-0
1-甲氧基-2-(3-甲基-3-丁烯-1-基)苯
反应条件
1: methoxybenzene With 3,4,5,6-tetrachloro-1,2-benzoquinone; [CpMoCl(CO)3] T=20°C; Friedel Crafts-type alkylation; 0.5 h; Inert atmosphere; 2: 3,3-dimethylallyl alcohol T=60°C; Friedel Crafts-type alkylation; 6 h; Inert atmosphere;
参考文献
Yamamoto, Yoshihiko; Itonaga, Kouhei
Chemistry - A European Journal, 2008 , vol. 14, # 34 p. 10705 - 10715
556-82-1
异戊烯醇
→
反应条件
21343-40-8
25-羟基维生素 D2
反应条件
1: 25 percent / tert-butylhydroperoxide, titanium(IV) isopropoxyde, D-(-)-dibutyl tartarate / CH2Cl2 / -20 °C 2: 92 percent / NaH / dimethylsulfoxide / Ambient temperature 3: 93 percent / diethyl ether / -20 °C 5: 90 percent / pyridine 6: 91 percent / potassium tert-butylate / dimethylformamide 7: 99 percent / Na2WO4, H2O2 / 70 °C 8: 95 percent / pyridinium p-toluenesulphonate / CH2Cl2 9: 1) lithium diisopropylamide / 1) THF, -78 deg C 10: 52 percent / 5percent Na-Hg, Na2HPO4 / 0 °C 11: 95 percent / 95percent ethanol / pyridinium p-toluenesulphonate / 40 °C 12: irradiation followed by thermal isomerization View Scheme
参考文献
Yamada, Sachiko; Shiraishi, Masami; Ohmori, Masayuki; Takayama, Hiroaki
Tetrahedron Letters, 1984 , vol. 25, # 31 p. 3347 - 3350
201230-82-2
+
55-21-0
+
556-82-1
异戊烯醇
→
反应条件
1466-83-7
反应条件
hydrogen; RhH(CO)(triphenylphosphine)3; dicobalt octacarbonyl in 1,4-dioxane T=110°C; P=60800 - 83600.1 Torr; 12 h;
参考文献
Hirai, Kenji; Takahashi, Yoshitaka; Ojima, Iwao
Tetrahedron Letters, 1982 , vol. 23, # 24 p. 2491 - 2494
556-82-1
异戊烯醇
+
126-84-1
→
反应条件
16647-04-4
反应条件
toluene-4-sulfonic acid; hydroquinone in benzene
参考文献
Kuznetsov,N.V.; Svishchuk,A.A.
Sov. Prog. Chem. (Engl. Transl.), 1966 , vol. 32, p. 725 - 727,559 - 560
100-66-3
苯甲醚
+
556-82-1
异戊烯醇
→
反应条件
4957-18-0
+
4957-17-9
+
18491-21-9
+
18272-85-0
1-甲氧基-2-(3-甲基-3-丁烯-1-基)苯
反应条件
1: methoxybenzene With 3,4,5,6-tetrachloro-1,2-benzoquinone; [CpMoCl(CO)3] T=20°C; Friedel Crafts-type alkylation; 0.5 h; Inert atmosphere; 2: 3,3-dimethylallyl alcohol T=60°C; Friedel Crafts-type alkylation; 6 h; Inert atmosphere;
参考文献
Yamamoto, Yoshihiko; Itonaga, Kouhei
Chemistry - A European Journal, 2008 , vol. 14, # 34 p. 10705 - 10715
331-39-5
+
556-82-1
异戊烯醇
→
反应条件
118971-61-2
反应条件
di-isopropyl azodicarboxylate; thiamine diphosphate in tetrahydrofuran T=20°C; Mitsunobu esterification;
参考文献
Appendino, Giovanni; Minassi, Alberto; Daddario, Nives; Bianchi, Federica; Tron, Gian Cesare
Organic Letters, 2002 , vol. 4, # 22 p. 3839 - 3841
52791-88-5
+
556-82-1
异戊烯醇
→
反应条件
112607-91-7
反应条件
tetraethylammonium p-toluenesulfonate in acetonitrile below 5 deg C, anodic oxidation with graphite anode and platinum cathode;
参考文献
Koizumi, Toshio; Fuchigami, Toshio; Nonaka, Tsutomu
Chemistry Letters, 1987 , p. 1095 - 1096
556-82-1
异戊烯醇
→
反应条件
117983-12-7
反应条件
1: 1) NaH / 1) THF, 2) room temperature, 1 h 2: 43 percent / BCl3 / pentane; hexane / 1 h / Ambient temperature 3: 44 percent / tetrahydrofuran; dimethylformamide View Scheme
参考文献
Bedford; Harris III; Howd; Goff; Koolpe; Petesch; Koplovitz; Sultan; Musallam
Journal of Medicinal Chemistry, 1989 , vol. 32, # 2 p. 504 - 516
51632-16-7
+
556-82-1
异戊烯醇
→
反应条件
113312-83-7
反应条件
sodium hydride 1) benzene, reflux, 2 h, 2) benzene, reflux, 8 h; Yield given. Multistep reaction;
参考文献
Joshi, G. S.; Kulkarni, G. H.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 445 - 447
556-82-1
异戊烯醇
→
反应条件
36971-12-7
反应条件
1: 46 percent / FeBr2; 2,2'-bipyridine; Bu4NBF4 / dimethylformamide / 20 °C / Electrochemical reaction View Scheme
参考文献
Durandetti, Muriel; Meignein, Clotilde; Perichon, Jacques
Journal of Organic Chemistry, 2003 , vol. 68, # 8 p. 3121 - 3124
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