1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C
1.2: 1.33 h / -78 - 20 °C / Inert atmosphere
2.1: water; potassium hydroxide / acetonitrile / 4 h / 60 °C / Inert atmosphere
View Scheme
参考文献
Ebner, Christian; Mueller, Constanze A.; Markert, Christian; Pfaltz, Andreas
Journal of the American Chemical Society, 2011 , vol. 133, # 13 p. 4710 - 4713