1,2-二甲氧基-6-甲基-4H-二苯并[de,g]喹啉-4,5(6H)-二酮合成路线 （共 9 条）
反应条件
tin(IV) chloride in dichloromethane
T=60°C; 24 h;
参考文献
Suau; Rico; Najera; Ortiz-Lopez; Lopez-Romero; Moreno-Manas; Roglans
Tetrahedron, 2004 , vol. 60, # 27 p. 5725 - 5735
反应条件
sodium hydride in ethylene glycol dimethyl ether
2 h;
参考文献
Atanes, N.; Castedo, L.; Guitian, E.; Saa, C.; Saa, J. M.; Suau, R.
Journal of Organic Chemistry, 1991 , vol. 56, # 9 p. 2984 - 2988
反应条件
sodium hydride in N,N-dimethyl-formamide
参考文献
Castedo, Luis; Guitian, Enrique; Saa, Jose M.; Suau, Rafael
Tetrahedron Letters, 1982 , vol. 23, # 4 p. 457 - 458
反应条件
air in water; acetonitrile
4 h; Irradiation;
参考文献
Suau, Rafael; Lopez-Romero, Juan Manuel; Rico, Rodrigo; Alonso, Francisco J.; Lobo, Carolina
Tetrahedron, 1996 , vol. 52, # 34 p. 11307 - 11320
反应条件
1: 62 percent / aq. NaHSO3 / 18 h / 150 °C
2: 59 percent / aq. NaOH / CH2Cl2 / 1 h / Ambient temperature
3: 31 percent / air / acetonitrile; H2O / 4 h / Irradiation
View Scheme
参考文献
Suau, Rafael; Lopez-Romero, Juan Manuel; Rico, Rodrigo; Alonso, Francisco J.; Lobo, Carolina
Tetrahedron, 1996 , vol. 52, # 34 p. 11307 - 11320
反应条件
1: 59 percent / aq. NaOH / CH2Cl2 / 1 h / Ambient temperature
2: 31 percent / air / acetonitrile; H2O / 4 h / Irradiation
View Scheme
参考文献
Suau, Rafael; Lopez-Romero, Juan Manuel; Rico, Rodrigo; Alonso, Francisco J.; Lobo, Carolina
Tetrahedron, 1996 , vol. 52, # 34 p. 11307 - 11320
反应条件
1: 87 percent / aq. HCl / tetrahydrofuran / 12 h / 60 °C
2: 62 percent / aq. NaHSO3 / 18 h / 150 °C
3: 59 percent / aq. NaOH / CH2Cl2 / 1 h / Ambient temperature
4: 31 percent / air / acetonitrile; H2O / 4 h / Irradiation
View Scheme
参考文献
Suau, Rafael; Lopez-Romero, Juan Manuel; Rico, Rodrigo; Alonso, Francisco J.; Lobo, Carolina
Tetrahedron, 1996 , vol. 52, # 34 p. 11307 - 11320
反应条件
oxalyl dichloride; tin(IV) chloride
1.) CH2Cl2, 20 deg C, 30 min, 2.) CH2Cl2, 20 deg C, 48 h; Yield given. Multistep reaction;
参考文献
Suau, Rafael; Lopez-Romero, Juan Manuel; Rico, Rodrigo
Tetrahedron, 1997 , vol. 53, # 42 p. 14397 - 14410
反应条件
tin(IV) chloride
1.) CH2Cl2, 20 deg C, 15 min, 2.) CH2Cl2, 5 deg C, 72 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Suau, Rafael; Lopez-Romero, Juan Manuel; Rico, Rodrigo
Tetrahedron, 1997 , vol. 53, # 42 p. 14397 - 14410
