三-O-苄基-D-葡萄烯糖合成路线 （共 122 条）
反应条件
sodium acetate; copper; acetic acid; zinc in tetrahydrofuran T=0 - 20°C; 3 h;
参考文献
Boutureira, Omar; Rodriguez, Miguel Angel; Matheu, M. Isabel; Diaz, Yolanda; Castillon, Sergio
Organic Letters, 2006 , vol. 8, # 4 p. 673 - 675
反应条件
1: 2,3,4,6-Tetra-O-benzyl-α-D-mannopyranosyl chloride With N,N-dimethylimidazolone; ethylene glycol dimethyl ether; nickel dichloride T=20°C; 0.333333 h; 2: (2-(1,3-dioxolan-2-yl)ethyl)zinc(II) bromide 12 h;
参考文献
Journal of the American Chemical Society, , vol. 129, # 7 p. 1908 - 1909
反应条件
ethylene glycol dimethyl ether; nickel dichloride; Pybox in 1,3-dimethyl-imidazolidin-2-one; ethylene glycol dimethyl ether T=25°C; Negishi coupling reaction; 12 h;
参考文献
Journal of the American Chemical Society, , vol. 130, # 36 p. 12177 - 12183
反应条件
samarium diiodide in tetrahydrofuran T=20°C; 0.166667 h;
参考文献
Angewandte Chemie, , vol. 107, # 8 p. 990 - 993
反应条件
manganese; chloro-trimethyl-silane; bis(cyclopentadienyl)titanium dichloride in tetrahydrofuran T=20°C; 12 h;
参考文献
Hansen; Daasbjerg; Skrydstrup
Tetrahedron Letters, 2000 , vol. 41, # 44 p. 8645 - 8649
反应条件
1: 2,3,4,6-Tetra-O-benzyl-α-D-mannopyranosyl chloride With N,N-dimethylimidazolone; ethylene glycol dimethyl ether; nickel dichloride T=20°C; 0.333333 h; 2: C11H10BrNO2Zn 12 h;
参考文献
Journal of the American Chemical Society, , vol. 129, # 7 p. 1908 - 1909
反应条件
ethylene glycol dimethyl ether; nickel dichloride; Pybox in 1,3-dimethyl-imidazolidin-2-one; ethylene glycol dimethyl ether T=25°C; Negishi coupling reaction; 12 h;
参考文献
Journal of the American Chemical Society, , vol. 130, # 36 p. 12177 - 12183
反应条件
samarium diiodide in tetrahydrofuran T=20°C; 1.5 h;
参考文献
Skrydstrup, Troels; Mazeas, Daniel; Elmouchir, Mohamed; Doisneau, Gilles; Riche, Claude; Chiaroni, Angele; Beau, Jean-Marie
Chemistry - A European Journal, 1997 , vol. 3, # 8 p. 1342 - 1356
反应条件
samarium diiodide in tetrahydrofuran T=20°C;
参考文献
Skrydstrup, Troels; Mazeas, Daniel; Elmouchir, Mohamed; Doisneau, Gilles; Riche, Claude; Chiaroni, Angele; Beau, Jean-Marie
Chemistry - A European Journal, 1997 , vol. 3, # 8 p. 1342 - 1356
反应条件
1: 2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl chloride With N,N-dimethylimidazolone; ethylene glycol dimethyl ether; nickel dichloride T=20°C; 0.333333 h; 2: bromo(4-ethoxy-4-oxobutyl)zinc 12 h;
参考文献
Journal of the American Chemical Society, , vol. 129, # 7 p. 1908 - 1909
