三-O-苄基-D-葡萄烯糖合成路线 (共 122 条)
反应条件
samarium diiodide; cyclohexanone in tetrahydrofuran T=20°C; 0.166667 h;
参考文献
Chemistry - A European Journal, , vol. 4, # 4 p. 655 - 671
反应条件
samarium diiodide in tetrahydrofuran T=25°C;
参考文献
Angewandte Chemie, , vol. 108, # 22 p. 2829 - 2832
反应条件
1: 99 percent / Et3N, DMAP / CH2Cl2 / 0.33 h / 20 °C 2: 1.) SmI2, 2.) Bu4NF / 1.) THF, 20 deg C, 10 min, 2.) THF, 0 deg C, 5 min View Scheme
参考文献
Chemistry - A European Journal, , vol. 4, # 4 p. 655 - 671
反应条件
potassium; carbon in tetrahydrofuran 5 h; Ambient temperature;
参考文献
Fuerstner, Alois
Liebigs Annalen der Chemie, 1993 , # 11 p. 1211 - 1218
反应条件
1: 94 percent / Et3N, DMAP / CH2Cl2 / 0.17 h / 20 °C 2: 1.) SmI2, 2.) Bu4NF / 1.) THF, 20 deg C, 10 min, 2.) THF, 0 deg C, 5 min View Scheme
参考文献
Chemistry - A European Journal, , vol. 4, # 4 p. 655 - 671
反应条件
1: 78 percent / HgBr2 / acetonitrile / 2 h / Heating 2: 64 percent / SmI2 / tetrahydrofuran / 1.5 h / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 3, # 8 p. 1342 - 1356
反应条件
1: 1 M sodium methoxide / methanol 2: 74 percent / sodium hydride / dimethylformamide / 12 h View Scheme
参考文献
Carbohydrate Research, , vol. 98, p. 25 - 36
反应条件
samarium diiodide in tetrahydrofuran T=20°C; 0.166667 h;
参考文献
Angewandte Chemie, , vol. 107, # 8 p. 990 - 993
反应条件
samarium diiodide in tetrahydrofuran Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 39, # 21 p. 3477 - 3480
反应条件
1: With N,N-dimethyl-formamide in chloroform-d1 T=0°C; 2: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate in chloroform-d1 T=0°C; Temperature;
参考文献
European Journal of Organic Chemistry, , vol. 2014, # 9 p. 1827 - 1831