三-O-苄基-D-葡萄烯糖合成路线 (共 122 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 2 h; Heating;
参考文献
Journal of Carbohydrate Chemistry, , vol. 20, # 3-4 p. 257 - 262
反应条件
1: Pd(OAc)2; 1,10-phenanthroline / CH2Cl2 / 72 h / Heating 2: Grubbs catalyst / CH2Cl2 / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 44, # 21 p. 4057 - 4061
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 3 h; Heating;
参考文献
Journal of Carbohydrate Chemistry, , vol. 20, # 3-4 p. 257 - 262
反应条件
1: oxone(R) / methanol; tetrahydrofuran; H2O / 0 °C 2: benzene / 1.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 67, # 17 p. 6195 - 6209
反应条件
1: acetic acid; zinc / water / -20 - 0 °C / Inert atmosphere 2: methanol; sodium methylate / 20 °C / Inert atmosphere 3: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 60 °C / Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 14, # 1 p. 174 - 177
反应条件
1: hydrogen bromide; acetic acid / 12 h / 20 °C / Inert atmosphere 2: acetic acid; zinc / water / -20 - 0 °C / Inert atmosphere 3: methanol; sodium methylate / 20 °C / Inert atmosphere 4: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 60 °C / Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 14, # 1 p. 174 - 177
反应条件
naphthalenyllithium in tetrahydrofuran T=-78°C; 0.25 h; Yield given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 6 p. 355 - 356
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran Ambient temperature;
参考文献
Bulletin de la Societe Chimique de France, , vol. 130, # 3 p. 256 - 265
反应条件
1-(benzenesulfonyl)-2-lithioindole in tetrahydrofuran T=-78 - 20°C; Elimination;
参考文献
Polish Journal of Chemistry, , vol. 74, # 11 p. 1589 - 1598
反应条件
bis(tricyclohexylphosphine)benzylidene ruthenium(IV) dichloride in dichloromethane ring closing metathesis; Heating;
参考文献
Peczuh, Mark W.; Snyder, Nicole L.
Tetrahedron Letters, 2003 , vol. 44, # 21 p. 4057 - 4061