三-O-苄基-D-葡萄烯糖合成路线 （共 122 条）
反应条件
[Cp2Ti(III)Cl]2 in tetrahydrofuran 0.25 h; Ambient temperature;
参考文献
Spencer, Roxanne P.; Cavallaro, Cullen L.; Schwartz, Jeffrey
Journal of Organic Chemistry, 1999 , vol. 64, # 11 p. 3987 - 3995
反应条件
2: 94 percent / <Cp2TiCl>2 / tetrahydrofuran / 0.25 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 64, # 11 p. 3987 - 3995
反应条件
1: PhSH, BF3*OEt2 / CH2Cl2 / -78 deg C -> room temperature 2: Oxone / methanol; tetrahydrofuran; H2O 3: benzene / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 61, # 20 p. 6754 - 6755
反应条件
1: PhSH, BF3*OEt2 / CH2Cl2 / -78 deg C -> room temperature 2: Oxone / methanol; tetrahydrofuran; H2O 3: benzene / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 61, # 20 p. 6754 - 6755
反应条件
1: 75 percent / SmI2 / tetrahydrofuran; methanol / a) -78 deg C to -40 deg C, 1 h, b) -40 deg C, 1 h 2: 89 percent / s-collidine, methanesulfonic anhydride (Ms2O) / CH2Cl2 / 6 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 4 p. 933 - 936
反应条件
2: 75 percent / SmI2 / tetrahydrofuran; methanol / a) -78 deg C to -40 deg C, 1 h, b) -40 deg C, 1 h 3: 89 percent / s-collidine, methanesulfonic anhydride (Ms2O) / CH2Cl2 / 6 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 4 p. 933 - 936
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 39, # 21 p. 3477 - 3480
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran 24 h; Ambient temperature;
参考文献
Bulletin de la Societe Chimique de France, , vol. 130, # 3 p. 256 - 265
反应条件
nickel in tetrahydrofuran; ethanol
参考文献
Bioorganic and Medicinal Chemistry, , vol. 10, # 2 p. 273 - 281
参考文献
Journal of Organic Chemistry, , vol. 61, # 20 p. 6754 - 6755
