in neat (no solvent)
byproducts: CF3I; carried out under inert atm.; freshly sublimed GeI4 and Te-compd. allowed to interact at 170°C for 120h, or for 150h at 120, 140 and 150°C; not isolated, monitored by NMR;
参考文献
Ganja, E. A.; Morrison, J. A.
Inorganic Chemistry, 1990 , vol. 29, p. 33 - 38
in neat (no solvent)
react. of Pb(CH3)4 (0.5 mmol) with (CF3)4Ge (2 mmol) in glass-ampoule (sealed under high vac.) at 50°C;; not isolated, identified by 19F-NMR;;
参考文献
Eujen, R.; Patorra, A.
Journal of Organometallic Chemistry, 1992 , vol. 438, # 1.2 p. 57 - 75
in neat (no solvent)
react. of Pb(CH3)4 (0.5 mmol) with (CF3)4Ge (2 mmol) in glass-ampoule (sealed under high vac.) at 50°C;; not isolated, identified by 19F-NMR;;
参考文献
Eujen, R.; Patorra, A.
Journal of Organometallic Chemistry, 1992 , vol. 438, # 1.2 p. 57 - 75
