2-苯基-1,2,3,4-四氢异喹啉-1-甲腈合成路线 （共 15 条）
反应条件
ruthenium trichloride; oxygen; acetic acid in methanol
T=60°C; P=760 Torr;
参考文献
Murahashi, Shun-Ichi; Komiya, Naruyoshi; Terai, Hiroyuki; Nakae, Takahiro
Journal of the American Chemical Society, 2003 , vol. 125, # 50 p. 15312 - 15313
反应条件
oxygen; acetic acid in methanol
T=20°C; 5 h; Irradiation; Catalytic behavior;
参考文献
Kumar, Pawan; Varma, Sanny; Jain, Suman L.
Journal of Materials Chemistry A, 2014 , vol. 2, # 13 p. 4514 - 4519
反应条件
tert.-butylhydroperoxide; [AubpyCl2]Cl in methanol; decane
T=20°C; 5 h; regioselective reaction;
参考文献
Zhang, Yan; Peng, Hao; Zhang, Ming; Cheng, Yixiang; Zhu, Chengjian
Chemical Communications, 2011 , vol. 47, # 8 p. 2354 - 2356
反应条件
2,4,5,7-tetrabromofluorescein in N,N-dimethyl-formamide
T=20°C; 10 h; Irradiation;
参考文献
Hari, Durga Prasad; Koenig, Burkhard
Organic Letters, 2011 , vol. 13, # 15 p. 3852 - 3855
反应条件
silica gel; 2,3-dicyano-5,6-dichloro-p-benzoquinone
T=20°C; 0.5 h; ball millingneat (no solvent);
参考文献
Su, Weike; Yu, Jingbo; Li, Zhenhua; Jiang, Zhijiang
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 9144 - 9150
反应条件
dihydrogen peroxide; ruthenium trichloride in methanol; water
T=20°C; 4 h;
参考文献
Murahashi, Shun-Ichi; Komiya, Naruyoshi; Terai, Hiroyuki
Angewandte Chemie - International Edition, 2005 , vol. 44, # 42 p. 6931 - 6933
反应条件
ruthenium trichloride; dihydrogen peroxide in methanol; water
T=50°C; 3 h;
参考文献
Verma, Sanny; Jain, Suman L.; Sain, Bir
Catalysis Letters, 2011 , vol. 141, # 6 p. 882 - 885
反应条件
[Ir(tbp-py)2(bpy)]PF6; acetic acid in acetonitrile
Strecker reaction; 20 h; Irradiation;
参考文献
Rueping, Magnus; Zhu, Shaoqun; Koenigs, Rene M.
Chemical Communications, 2011 , vol. 47, # 47 p. 12709 - 12711
反应条件
1: copper(l) iodide; potassium phosphate / ethylene glycol; isopropyl alcohol / 24 h / 20 - 90 °C / Inert atmosphere
2: 2,4,5,7-tetrabromofluorescein / N,N-dimethyl-formamide / 10 h / 20 °C / Irradiation
View Scheme
参考文献
Hari, Durga Prasad; Koenig, Burkhard
Organic Letters, 2011 , vol. 13, # 15 p. 3852 - 3855
反应条件
1: copper(l) iodide; potassium phosphate / ethylene glycol; isopropyl alcohol / 24 h / 20 - 90 °C / Inert atmosphere
2: 2,4,5,7-tetrabromofluorescein / N,N-dimethyl-formamide / 10 h / 20 °C / Irradiation
View Scheme
参考文献
Hari, Durga Prasad; Koenig, Burkhard
Organic Letters, 2011 , vol. 13, # 15 p. 3852 - 3855
