N-ethyl-N,N-diisopropylamine; trichlorophosphate in toluene
T=110°C;
参考文献
Dudash Jr., Joseph; Zhang, Yongzheng; Moore, John B.; Look, Richard; Liang, Yin; Beavers, Mary Pat; Conway, Bruce R.; Rybczynski, Philip J.; Demarest, Keith T.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 21 p. 4790 - 4793
1: 71 percent / Et3N / CH2Cl2 / 20 °C
2: 83 percent / phosphorous oxychloride; Huning's base / toluene / 110 °C
View Scheme
参考文献
Dudash Jr., Joseph; Zhang, Yongzheng; Moore, John B.; Look, Richard; Liang, Yin; Beavers, Mary Pat; Conway, Bruce R.; Rybczynski, Philip J.; Demarest, Keith T.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 21 p. 4790 - 4793