反应条件
1: 1.) sodium hydride / 1.) DMF, 45 min, 65 deg C; 2.) THF-DMF, 60 deg C, 20 min
2: 58 percent / amalgamated alumina / tetrahydrofuran; H2O / 5 h / 60 °C
3: 80 percent / hydroxylamine hydrochloride, pyridine / ethanol / 4 h / Heating
View Scheme
参考文献
Kompis; Then; Boehni; et al.
European Journal of Medicinal Chemistry, 1980 , vol. 15, # 1 p. 17 - 22
