1: With (S)-bis(3,5-dimethylphenyl)(1-methylpyrrolidin-2-yl)methanol in hexane; toluene T=20°C; 10 h; Inert atmosphere; 2: With ammonium chloride in hexane; toluene optical yield given as percent eeenantioselective reaction;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 12 p. 4425 - 4428
1: 4-iodobenzoic acid ethyl ester; diethylzinc With t-Bu-N=P[N=P(NMe)3]3 in tetrahydrofuran; hexane T=20°C; 5 h; 2: benzaldehyde in tetrahydrofuran; hexane T=-40 - 20°C; 17 h; Further stages. Title compound not separated from byproducts.;
参考文献
Ueno, Masahiro; Wheatley, Andrew E. H.; Kondo, Yoshinori
Chemical Communications, 2006 , # 33 p. 3549 - 3550
