1-methyl-pyrrolidin-2-one; tetrabutylammomium bromide; nickel dichloride; buta-1,3-diene in tetrahydrofuran; hexane T=25°C; 48 h; Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 45 p. 6180 - 6182
1: diethylzinc; phenylacetylene With chiral bicyclo[3.2.1]octane-based alcohol in tetrahydrofuran; hexane 1 h; 2: 3-chloro-benzaldehyde in tetrahydrofuran; hexane T=0°C; 6 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Scarpi, Dina; Galbo, Fabrizio Lo; Guarna, Antonio
Tetrahedron Asymmetry, 2006 , vol. 17, # 9 p. 1409 - 1414