1-methyl-pyrrolidin-2-one; tetrabutylammomium bromide; nickel dichloride; buta-1,3-diene in tetrahydrofuran; hexane T=25°C; 48 h; Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 45 p. 6180 - 6182
1: 2-methyl-2-propenal; diethylzinc With (1R,2S)-(+)-1-cyclohexyl-2-phenyl-2-(N-morpholino)ethanol in hexane; toluene T=20°C; 3 h; 2: acetic anhydride in hexane; toluene Further stages. Title compound not separated from byproducts.;
参考文献
Nugent, William A.
Organic Letters, 2002 , vol. 4, # 13 p. 2133 - 2136