1: 2-(benzyloxyimino)ethanoic acid With 4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide; Wang resin in dichloromethane
T=20°C; 12 h;
2: diethylzinc in hexane; dichloromethane
T=-78°C;
3: With trifluoroacetic acid in chloroform
T=20°C; 0.5 h;
Crist, DeLanson R.; Jordan, Guy J.; Moore, Donald W.; Hashmall, Joseph A.; Borsetti, Arnold P.; Turujman, Saleh A.
Journal of the American Chemical Society, 1983 , vol. 105, # 13 p. 4136 - 4142
copper; ammonium chloride; zinc
1) benzene, hexane, a) 0 deg C, 3 h, b) r.t., 19 h, 2) MeOH, r.t., 2.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Mann, John; Barbosa, Luiz-Claudio de Almeida
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 7 p. 787 - 790
durch Zersetzen des Reaktionsproduktes mit Wasser;
参考文献
Frankland; Duppa
Justus Liebigs Annalen der Chemie, 1865 , vol. 135, p. 26
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Frankland
Justus Liebigs Annalen der Chemie, 1863 , vol. 126, p. 109