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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
氰化锌
合成路线
（共 506 条）
51417-51-7
7-溴吲哚
+
557-21-1
氰化锌
→
反应条件
96631-87-7
7-氰基吲哚
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=170°C; 0.25 h; Microwave reactor;
参考文献
ACADIA PHARMACEUTICALS INC.
Patent: WO2007/79239 A2, 2007 ;
Location in patent: Page/Page column 99-100 ;
WO 2007/079239 A2
557-21-1
氰化锌
+
51417-51-7
7-溴吲哚
→
反应条件
96631-87-7
7-氰基吲哚
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=170°C; 0.333333 h; Microwave irradiation;
参考文献
Castro Pineiro, Jose Luis; Lin, Xichen; Liu, Qian; Meng, Kevin; Ren, Feng; Vesey, David R.; Zhao, Baowei
Patent: US2010/29729 A1, 2010 ;
Location in patent: Page/Page column 15 ;
557-21-1
氰化锌
+
2051-62-9
4-氯联苯
→
反应条件
2920-38-9
4-氰基联苯
反应条件
sulfuric acid; palladium diacetate; zinc; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in dimethylammonium 2,4-dichlorophenoxyacetate T=120°C; 2 h; Inert atmosphere;
参考文献
Shevlin, Michael
Tetrahedron Letters, 2010 , vol. 51, # 37 p. 4833 - 4836
591-20-8
间溴苯酚
+
557-21-1
氰化锌
→
反应条件
873-62-1
3-氰基苯酚
反应条件
water; [(t-Bu)3PH]BF4; zinc; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in 1-methyl-pyrrolidin-2-one T=80°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 46, # 11 p. 1815 - 1818
16110-09-1
2,5-二氯吡啶
+
557-21-1
氰化锌
→
反应条件
89809-64-3
5-氯-2-氰基吡啶
反应条件
zinc; bis(diphenylphosphino)dipalladium (II) CH2Cl2 complex T=160 - 185°C;
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/66126 A1, 2005 ;
Location in patent: Page/Page column 74-75 ;
WO 2005/066126 A1
624-28-2
2,5-二溴吡啶
+
557-21-1
氰化锌
→
反应条件
97483-77-7
5-溴-2-氰基吡啶
反应条件
zinc; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in dichloromethane; N,N-dimethyl-formamide 5 h; Heating / reflux;
参考文献
IRM LLC
Patent: US2007/203100 A1, 2007 ;
Location in patent: Page/Page column 11 ;
452-74-4
4-溴-3-氟甲苯
+
557-21-1
氰化锌
→
反应条件
85070-67-3
2-氟-4-甲基苯甲腈
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=80°C;
参考文献
Dinsmore; Bogusky; Culberson; Bergman; Homnick; Zartman; Mosser; Schaber; Robinson; Koblan; Huber; Graham; Hartman; Huff; Williams
Journal of the American Chemical Society, 2001 , vol. 123, # 9 p. 2107 - 2108
203302-92-5
3-溴-2-氯-6-氟甲苯
+
557-21-1
氰化锌
→
反应条件
796600-15-2
2-氯-3-甲基-4-氟苯甲腈
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=120°C; 2 h; Product distribution / selectivity;
参考文献
Schlienger, Nathalie; Thygesen, Mikkel Boas; Pawlas, Jan; Badalassi, Fabrizio; Lewinsky, Rasmus; Lund, Birgitte Winther; Olsson, Roger
Patent: US2006/160845 A1, 2006 ;
Location in patent: Page/Page column 19 ;
557-21-1
氰化锌
+
5326-38-5
2-碘-5-硝基甲苯
→
反应条件
89001-53-6
2-甲基-4-硝基苯甲腈
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=120°C; 24 h;
参考文献
GRÜNENTHAL GMBH; FRANK, Robert; BAHRENBERG, Gregor; CHRISTOPH, Thomas; LESCH, Bernhard; LEE, Jeewoo
Patent: WO2013/45451 A1, 2013 ;
Location in patent: Page/Page column 80 ;
5326-38-5
2-碘-5-硝基甲苯
+
557-21-1
氰化锌
→
反应条件
89001-53-6
2-甲基-4-硝基苯甲腈
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=120°C; 24 h;
参考文献
GRÜNENTHAL GMBH; FRANK, Robert; BAHRENBERG, Gregor; CHRISTOPH, Thomas; LESCH, Bernhard; LEE, Jeewoo
Patent: WO2013/45447 A1, 2013 ;
Location in patent: Page/Page column 67 ;
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