反-2-,顺-6-壬二烯醛合成路线 (共 28 条)
反应条件
1: 66 percent 2: 64 percent / H2 / 5percent Pd-BaSO4 / ethyl acetate / 3 h 3: 25 percent / H2SO4 / acetone / 1 h / 70 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 3 p. 567 - 575
反应条件
1: palladium/calcium carbonate; ethyl acetate / Hydrogenation 2: chromium (VI)-oxide; aqueous sulfuric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 74, p. 4040,4042
反应条件
1: 65 percent / NACAA / CH2Cl2; pyridine / 0.33 h / 20 °C 2: benzene / Heating View Scheme
参考文献
Tetrahedron, , vol. 59, # 4 p. 567 - 573
反应条件
Dess-Martin periodane in dichloromethane T=20°C; 0.5 h;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 59, # 8 p. 4057 - 4061
反应条件
1: 74 percent / conc. H2SO4 / acetone; H2O / 20 °C 2: 65 percent / NACAA / CH2Cl2; pyridine / 0.33 h / 20 °C 3: benzene / Heating View Scheme
参考文献
Tetrahedron, , vol. 59, # 4 p. 567 - 573
反应条件
1: 70 percent / LAH, EtOH / diethyl ether 2: 52 percent / pyridinium chlorochromate, NaOAc / CH2Cl2 / 4 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 24, p. 313 - 314
反应条件
hydrogenchloride in methanol 18 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 3 p. 567 - 575
反应条件
1: aq. oxalic acid View Scheme
参考文献
Journal of Organic Chemistry, , vol. 38, p. 36 - 56
反应条件
in benzene Wittig reaction; Heating;
参考文献
Tetrahedron, , vol. 59, # 4 p. 567 - 573
反应条件
1: ueber nicht rein erhaltenes 1-Brom-nonadien-(2t.6c) und Nonadien-(2t.6c)-yl-benzoat 2: Cr2O3-H2SO4 View Scheme
参考文献
Chemische Berichte, , vol. 80, p. 141
Bulletin of the Agricultural Chemical Society of Japan, vol. 14, p. 65
Chem. Zentralbl., , vol. 109, # II p. 3696