(S)-1,1-二甲氧基-2-丙胺合成路线 （共 5 条）
反应条件
palladium 10 on activated carbon; hydrogen in methanol
T=20°C; P=760.051 Torr; 1.5 h; Inert atmosphere;
参考文献
Sugimoto, Kenji; Toyoshima, Kazuki; Nonaka, Shiori; Kotaki, Kenta; Ueda, Hirofumi; Tokuyama, Hidetoshi
Angewandte Chemie - International Edition, 2013 , vol. 52, # 28 p. 7168 - 7171
Angew. Chem., 2013 , vol. 125, # 28 p. 7309 - 7312,4
反应条件
ammonium formate; palladium on activated charcoal in methanol
1 h; Heating;
参考文献
Bringmann, Gerhard; Geisler, Joerg-Peter
Synthesis, 1989 , # 8 p. 608 - 610
反应条件
1: TsOH / toluene / Heating
2: H2 / Raney-Ni / ethanol / 24 h / 3750.3 Torr / Ambient temperature
3: 96 percent / HCO2NH4 / 10percent Pd/C / methanol / 1 h / Heating
View Scheme
参考文献
Bringmann, Gerhard; Geisler, Joerg-Peter
Synthesis, 1989 , # 8 p. 608 - 610
反应条件
1: H2 / Raney-Ni / ethanol / 24 h / 3750.3 Torr / Ambient temperature
2: 96 percent / HCO2NH4 / 10percent Pd/C / methanol / 1 h / Heating
View Scheme
参考文献
Bringmann, Gerhard; Geisler, Joerg-Peter
Synthesis, 1989 , # 8 p. 608 - 610
参考文献
Gacek,M.; Undheim,K.
Tetrahedron, 1974 , vol. 30, p. 4233 - 4237
