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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
55709-45-0
合成路线
（共 12 条）
624-38-4
1,4-二碘苯
+
106-45-6
4-甲苯硫酚
→
反应条件
55709-45-0
反应条件
copper(l) iodide; iron (III) acetylacetonate; potassium carbonate in dimethyl sulfoxide T=140°C; 48 h; Inert atmosphere;
参考文献
Qu, Xiaoming; Li, Tingyi; Zhu, Yan; Sun, Peng; Yang, Hailong; Mao, Jincheng
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 14 p. 5043 - 5046
624-38-4
1,4-二碘苯
+
103-19-5
对甲苯二硫醚
→
反应条件
55709-45-0
反应条件
copper(l) iodide; 3-(dimethylamino)-1-(2-hydroxyphenyl)-prop-2-en-1-one; caesium carbonate in ethanol T=80°C; 15 h; Green chemistry;
参考文献
Liu, Yunyun; Wang, Hang; Zhang, Jida; Wan, Jie-Ping; Wen, Chengping
RSC Advances, 2014 , vol. 4, # 37 p. 19472 - 19475
106-37-6
对二溴苯
+
106-45-6
4-甲苯硫酚
→
反应条件
55709-45-0
+
22865-54-9
反应条件
1: para-thiocresol With sodium in diethyl ether Heating; 2: p-bromophenyl bromide With Ni(Br)2(dppe) in ethylene glycol T=170°C; 16 h;
参考文献
Qian, Ding-Quan; Liu, Bo; Shine, Henry J.; Guzman-Jimenez, Ilse Y.; Whitmire, Kenton H.
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 3 p. 139 - 147
589-87-7
对溴碘苯
+
106-45-6
4-甲苯硫酚
→
反应条件
55709-45-0
反应条件
potassium phosphate; copper(l) iodide; N,N-dimethylaminoacetic acid in N,N-dimethyl-formamide T=120°C; 48 h;
参考文献
Deng, Wei; Zou, Yan; Wang, Ye-Feng; Liu, Lei; Guo, Qing-Xiang
Synlett, 2004 , # 7 p. 1254 - 1258
540-36-3
1,4-二氟苯
+
106-45-6
4-甲苯硫酚
→
反应条件
55709-45-0
反应条件
pyridine; quinoline; copper(I) oxide T=175°C; 25 h;
参考文献
Goyot, Olivier; Gingras, Marc
Tetrahedron Letters, 2009 , vol. 50, # 17 p. 1977 - 1981
106-45-6
4-甲苯硫酚
→
反应条件
55709-45-0
+
22865-54-9
反应条件
1: para-thiocresol With sodium in diethyl ether Heating; 2: 5-(p-bromophenyl)thianthrenium bromide in acetonitrile T=20°C;
参考文献
Qian, Ding-Quan; Liu, Bo; Shine, Henry J.; Guzman-Jimenez, Ilse Y.; Whitmire, Kenton H.
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 3 p. 139 - 147
106-45-6
4-甲苯硫酚
→
反应条件
55709-45-0
+
22865-55-0
反应条件
1: para-thiocresol With sodium in diethyl ether Heating; 2: 5-(p-chlorophenyl)thianthrenium bromide in acetonitrile T=20°C;
参考文献
Qian, Ding-Quan; Liu, Bo; Shine, Henry J.; Guzman-Jimenez, Ilse Y.; Whitmire, Kenton H.
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 3 p. 139 - 147
2362-50-7
噻蒽 5-氧化物
→
反应条件
55709-45-0
反应条件
1.1: 63 percent / benzene / Heating 2.1: Na / diethyl ether / Heating 2.2: 34 percent / acetonitrile / 20 °C View Scheme
参考文献
Qian, Ding-Quan; Liu, Bo; Shine, Henry J.; Guzman-Jimenez, Ilse Y.; Whitmire, Kenton H.
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 3 p. 139 - 147
873-77-8
4-氯苯基溴化镁
→
反应条件
55709-45-0
反应条件
1.1: 48 percent / benzene / Heating 2.1: Na / diethyl ether / Heating 2.2: 33 percent / acetonitrile / 20 °C View Scheme
参考文献
Qian, Ding-Quan; Liu, Bo; Shine, Henry J.; Guzman-Jimenez, Ilse Y.; Whitmire, Kenton H.
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 3 p. 139 - 147
18620-02-5
→
反应条件
55709-45-0
反应条件
1.1: 63 percent / benzene / Heating 2.1: Na / diethyl ether / Heating 2.2: 34 percent / acetonitrile / 20 °C View Scheme
参考文献
Qian, Ding-Quan; Liu, Bo; Shine, Henry J.; Guzman-Jimenez, Ilse Y.; Whitmire, Kenton H.
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 3 p. 139 - 147
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