3-(1,3-二噻烷-2-亚基)-2,4-戊二酮合成路线 （共 30 条）
反应条件
1: 92 percent / Mg / methanol / 24 h / 5 °C 2: 99 percent / NH2OH*HCl / ethanol / 2 h / Heating 3: 78 percent / NBS / H2O; acetonitrile / 0.17 h / -5 - 30 °C View Scheme
参考文献
Mellor, John M.; Schofield, Stephen R.; Korn, Stewart R.
Tetrahedron, 1997 , vol. 53, # 50 p. 17151 - 17162
反应条件
magnesium in methanol T=5°C; 24 h;
参考文献
Mellor, John M.; Schofield, Stephen R.; Korn, Stewart R.
Tetrahedron, 1997 , vol. 53, # 50 p. 17151 - 17162
反应条件
acetyl chloride in methanol 5.5 h; Heating;
参考文献
Yu, Haifeng; Liu, Qun; Yin, Yanbing; Fang, Qunxin; Zhang, Jingping; Dong, Dewen
Synlett, 2004 , # 6 p. 999 - 1002
反应条件
para-dodecylbenzenesulfonic acid in water 2.2 h; Heating;
参考文献
Dong, Dewen; Ouyang, Yan; Yu, Haifeng; Liu, Qun; Liu, Jun; Wang, Mang; Zhu, Jing
Journal of Organic Chemistry, 2005 , vol. 70, # 11 p. 4535 - 4537
反应条件
para-dodecylbenzenesulfonic acid in water 8 h; Heating;
参考文献
Ouyang, Yan; Dong, Dewen; Zheng, Chunbai; Yu, Haifeng; Liu, Qun; Fu, Zhenqian
Synthesis, 2006 , # 22 p. 3801 - 3804
反应条件
hydrogenchloride T=60°C; 1.33333 h;
参考文献
Ouyang, Yan; Dong, Dewen; Zheng, Chunbai; Yu, Haifeng; Liu, Qun; Fu, Zhenqian
Synthesis, 2006 , # 22 p. 3801 - 3804
反应条件
acetyl chloride in methanol
9 h; Heating;
参考文献
Yu, Haifeng; Liu, Qun; Yin, Yanbing; Fang, Qunxin; Zhang, Jingping; Dong, Dewen
Synlett, 2004 , # 6 p. 999 - 1002
反应条件
acetyl chloride in methanol
7 h; Heating;
参考文献
Yu, Haifeng; Liu, Qun; Yin, Yanbing; Fang, Qunxin; Zhang, Jingping; Dong, Dewen
Synlett, 2004 , # 6 p. 999 - 1002
反应条件
para-dodecylbenzenesulfonic acid in water
2.1 h; Heating;
参考文献
Dong, Dewen; Ouyang, Yan; Yu, Haifeng; Liu, Qun; Liu, Jun; Wang, Mang; Zhu, Jing
Journal of Organic Chemistry, 2005 , vol. 70, # 11 p. 4535 - 4537
反应条件
hydrogenchloride
T=60°C; 0.25 h;
参考文献
Ouyang, Yan; Dong, Dewen; Zheng, Chunbai; Yu, Haifeng; Liu, Qun; Fu, Zhenqian
Synthesis, 2006 , # 22 p. 3801 - 3804
