3,8-二甲基-5-异丙基-1,2-萘醌合成路线 （共 3 条）
反应条件
oxygen in chloroform
T=40°C; 240 h; Irradiation;
参考文献
Strunz, George M.; Yu, Chao-Mei; Salonius, Annalisa
Phytochemistry (Elsevier), 1989 , vol. 28, # 10 p. 2861 - 2863
反应条件
oxygen in chloroform
T=25°C; 24 h; Further byproducts given;
参考文献
Matsubara, Yoshiharu; Matsui, Shuichi; Takekuma, Shin-ichi; Quo, Yan Pin; Yamamoto, Hiroshi; Nozoe, Tetsuo
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 6 p. 2040 - 2044
反应条件
1.1: SeO2; t-BuOOH / CH2Cl2 / 36 h / 0 °C
1.2: NaBH4; MeOH / 1 h / 0 °C
2.1: DMAP / CH2Cl2 / 3 h / 0 °C
3.1: CF3CO2H; CH3CO2H / 12 h / 70 °C
3.2: 46 percent / BBr3 / CH2Cl2 / -78 - 20 °C
View Scheme
参考文献
Kraus, George A.; Jeon, Insik
Organic Letters, 2006 , vol. 8, # 23 p. 5315 - 5316
