甲基丙烯酰氧基甲基三乙氧基硅烷合成路线 (共 3 条)
反应条件
(10H)-phenothiazine; tetra-n-butyl phosphonium chloride T=108 - 112°C; P=75.0075 Torr; 4 h; Product distribution / selectivity;
参考文献
WACKER CHEMIE AG
Patent: US2012/4437 A1, 2012 ;
Location in patent: Page/Page column 4 ;
反应条件
1: 2-methyl-2-propenoic acid With potassium hydroxide in toluene 2: (chloromethyl)triethoxysilane With 4,4'-bismethylene(2,6-di-tert-butylphenol); tetra-n-butyl phosphonium chloride in toluene; butanone T=110°C; 4 h;
参考文献
Monatshefte fur Chemie, , vol. 134, # 8 p. 1081 - 1092
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 459,463; engl.Ausg.S.467,470