二甲基(2-硝基-1-苯基乙基)丙二酸酯合成路线 （共 15 条）
参考文献
Kohler, Engelbrecht
Journal of the American Chemical Society, 1919 , vol. 41, p. 766
反应条件
triethylamine; calcium chloride
T=20°C; Michael Addition; 0.5 h; Milling;
参考文献
Jia, Chunman; Chen, Da; Zhang, Chunyan; Zhang, Qi; Cao, Bennan; Zhao, Zhendong
Tetrahedron, 2013 , vol. 69, # 35 p. 7320 - 7324
反应条件
triethylamine
T=20°C; Michael Addition; Green chemistry;
参考文献
Agarwal, Jyoti; Naganaboina, Ram Tilak; Peddinli, Rama Krishna
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 4 p. 511 - 518
反应条件
microencapsulated poly(ethyleneimine); [(+/-)-trans-1,2-dibenzylaminocyclohexane]2*NiBr2 in methanol
T=20°C; 24 h;
参考文献
Poe, Sarah L.; Kobaslija, Muris; McQuade, D. Tyler
Journal of the American Chemical Society, 2007 , vol. 129, # 29 p. 9216 - 9221
反应条件
1: microencapsulated poly(ethyleneimine) catalyst / ethanol / 23.84 °C
2: [(+/-)-trans-1,2-dibenzylaminocyclohexane]*NiBr2 / microencapsulated poly(ethyleneimine) / methanol / 23.84 °C
View Scheme
参考文献
Poe, Sarah L.; Kobaslija, Muris; McQuade, D. Tyler
Journal of the American Chemical Society, 2007 , vol. 129, # 29 p. 9216 - 9221
反应条件
1: malonic acid dimethyl ester With potassium tert-butylate in tetrahydrofuran
T=0°C; 0.5 h;
2: (trans)-β-nitrostyrene With 4-(N,N-dimethlyamino)pyridine; phosphorus trichoride in tetrahydrofuran
0.5 h; Heating;
参考文献
Tu, Zhijay; Jang, Yaochung; Lin, Chunchi; Liu, Ju-Tsung; Hsu, Jianming; Sastry; Yao, Ching-Fa
Tetrahedron, 2005 , vol. 61, # 44 p. 10541 - 10551
反应条件
(trans-1,2-bis(N-benzylamino)cyclohexyl)NiBr2; poly(ethyleneimine) in methanol; toluene
T=20°C; 24 h;
参考文献
Poe, Sarah L.; Kobaslija, Muris; McQuade, D. Tyler
Journal of the American Chemical Society, 2006 , vol. 128, # 49 p. 15586 - 15587
反应条件
1: malonic acid dimethyl ester With potassium tert-butylate in tetrahydrofuran
T=0°C; 0.5 h;
2: (trans)-β-nitrostyrene With phosphorus trichoride in tetrahydrofuran
T=20°C; 1.5 h;
参考文献
Tu, Zhijay; Jang, Yaochung; Lin, Chunchi; Liu, Ju-Tsung; Hsu, Jianming; Sastry; Yao, Ching-Fa
Tetrahedron, 2005 , vol. 61, # 44 p. 10541 - 10551
参考文献
Kohler, Engelbrecht
Journal of the American Chemical Society, 1919 , vol. 41, p. 766
参考文献
Kohler, Engelbrecht
Journal of the American Chemical Society, 1919 , vol. 41, p. 766
