in solid matrix condensation of a stream of Li-atoms with CBr4 in an Ar-matrix at 15K on CsI (concn. Ar:CBr4 = 400-600, Li:CBr4 = 0.5-3);; determination by IR;;
参考文献
Andrews; Carver
Journal of Chemical Physics, 1968 , vol. 49, p. 896,897
in neat (no solvent) (N2); mixing of NaN(CN)2 and CBr4 in agate mortar in 1:4 ratio; grindingfor 5 min; placing in Cu container; pressing at 300 kg/cm**2 for 5 min; shock treatment (14 GPa); washing with water; monitoring by XRD;
参考文献
Shibata, Kazusato; Sekine, Toshimori
Solid State Communications, 2006 , vol. 139, # 10 p. 501 - 505
