3,3-二甲基-1-丁烯合成路线 （共 347 条）
反应条件
sodium hydroxide; sodium tetrahydroborate; Hg(NO3)2 1.) 5 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Brown, Herbert C.; Kurek, Joseph T.; Rei, Min-Hon; Thompson, Kerry L.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2551 - 2557
反应条件
sodium hydroxide; sodium tetrahydroborate; mercury(II) trifluoroacetate 1.) 1440 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Brown, Herbert C.; Kurek, Joseph T.; Rei, Min-Hon; Thompson, Kerry L.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2551 - 2557
反应条件
bromine; 2-methyl cyclohexane T=-60°C; und anschliessend mit Natriumamid in fluessigem Ammoniak bei -70grad;
参考文献
Miller et al.
Journal of Organic Chemistry, 1954 , vol. 19, p. 1882,1885,1887
反应条件
Erhitzen den entstehenden Dibromids mit KOH auf 200grad;
参考文献
Delacre
Chem. Zentralbl., 1906 , vol. 77, # II p. 498
参考文献
Nasarow et al.
Doklady Akademii Nauk SSSR, 1958 , vol. 118, p. 509
Doklady Chemistry, 118-123<1958>77
反应条件
3-methyl-2-amino-pyridine; Wilkinson's catalyst; 1-Hexylamine; α,α,α-Trifluoro-p-toluic acid; water in toluene T=150°C; 12 h;
参考文献
Cha, Kyung-Mi; Jo, Eun-Ae; Jun, Chul-Ho
Synlett, 2009 , # 18 p. 2939 - 2942
反应条件
1: zinc/copper couple; trichlorophosphate / diethyl ether / 40 °C 2: ammonium chloride; zinc / methanol / Reflux View Scheme
参考文献
Xu, Hua-Jian; Zhu, Feng-Fei; Shen, Yong-Ya; Wan, Xin; Feng, Yi-Si
Tetrahedron, 2012 , vol. 68, # 22 p. 4145 - 4151
反应条件
[(C6H6)(PCy3)(CO)RuH]+BF4- in chlorobenzene T=110°C; Autoclave;
参考文献
Lee, Dong-Hwan; Kwon, Ki-Hyeok; Yi, Chae S.
Science, 2011 , vol. 333, # 6049 p. 1613 - 1616
反应条件
aluminium trichloride; 2-Chloro-2-methylpropane; triisooctyl amine in 1,2-dichloro-ethane T=-8°C; 5 h; other olefin, var. solvents, and catalytic systems; Product distribution;
参考文献
Frank, Walter C.; Miller, Donna M.
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 1 p. 125 - 129
反应条件
1: 54 percent / tetrakis(triphenyl phosphite)nickel, triphenyl phosphite, ZnCl2 / toluene / 2.5 h / 60 °C 2: 65 percent / LiAlH4 / diethyl ether / 3 h / Heating View Scheme
参考文献
Australian Journal of Chemistry, , vol. 35, # 10 p. 2053 - 2067
