3,3-二甲基-1-丁烯合成路线 （共 347 条）
反应条件
lithium perchlorate in nitromethane T=20°C; Further byproducts given;
参考文献
Russian Journal of Organic Chemistry, , vol. 31, # 7 p. 943 - 951
Zhurnal Organicheskoi Khimii, , vol. 31, # 7 p. 1018 - 1026
反应条件
3-methyl-2-amino-pyridine; Wilkinson's catalyst; 1-Hexylamine; α,α,α-Trifluoro-p-toluic acid; water in toluene T=150°C; 24 h;
参考文献
Synlett, , # 18 p. 2939 - 2942
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=150°C; 12 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=150°C; 24 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., , vol. 126, # 5 p. 1414 - 1418
反应条件
P=5 - 150 Torr; Ambient temperatureIrradiationpresence/absence of oxygen, DI; Quantum yield;
参考文献
Deslauriers, Helene; Collin, Guy J.
Canadian Journal of Chemistry, 1985 , vol. 63, p. 62 - 67
反应条件
borane-ammonia complex; [Pd(N,N'-bis(2,6-diisopropylphenyl)imidazolidin-2-ylidene)(PCy3)] in isopropyl alcohol T=50°C; 16 h; Inert atmosphereGlovebox;
参考文献
Hartmann, Caroline E.; Jurcik, Vaclav; Songis, Olivier; Cazin, Catherine S. J.
Chemical Communications, 2013 , vol. 49, # 10 p. 1005 - 1007
反应条件
1: With [Ir(acetylacetonate)(1,5-cyclooctadiene)]; triphenylphosphine in N-methylpyrrolidone T=20 - 100°C; P=5250.53 Torr; Inert atmosphereAutoclave; 2: With hydrogen in N-methylpyrrolidone T=100°C; P=9750.98 Torr; 20 h; Autoclave; regioselective reaction;
参考文献
Piras, Irene; Jennerjahn, Reiko; Jackstell, Ralf; Spannenberg, Anke; Franke, Robert; Beller, Matthias
Angewandte Chemie - International Edition, 2011 , vol. 50, # 1 p. 280 - 284
反应条件
(1,10-phenanthroline)PdMe(OEt2)+Blt;3,5-C6H3(CF3)2gt;4- in dichloromethane T=25°C; 24 h; Yields of byproduct given;
参考文献
LaPointe, Anne M.; Rix, Francis C.; Brookhart, Maurice
Journal of the American Chemical Society, 1997 , vol. 119, # 5 p. 906 - 917
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=120°C; 12 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=120°C; 12 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
