3,3-二甲基-1-丁烯合成路线 (共 347 条)
反应条件
tert.-butyl lithium in diethyl ether; pentane T=-23°C; Title compound not separated from byproducts;
参考文献
Newcomb, Martin; Williams, William G.; Crumpacker, Elizabeth L.
Tetrahedron Letters, 1985 , vol. 26, # 9 p. 1183 - 1184
反应条件
tri-n-butyl-tin hydride; 2,2'-azo-bisisobutyronitrile in benzene 0.5 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 26, # 9 p. 1179 - 1182
反应条件
aluminium trichloride in benzene 2 h;
参考文献
Journal of the American Chemical Society, , vol. 102, p. 4515
反应条件
[(Et2N)3U][BPh4] in benzene-d6 T=78°C; hydrosilylation; 6 h; Further byproducts given;
参考文献
Journal of Organometallic Chemistry, , vol. 604, # 1 p. 83 - 98
反应条件
1: Ph3P, CBr4 / CH2Cl2 / 2 h / 0 - 25 °C 2: 13 percent / tert-butyllithium / diethyl ether; pentane / -23 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 26, # 9 p. 1183 - 1184
反应条件
T=25°C; P=650 Torr; 0.333333 h;
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 8 p. 1216 - 1220
反应条件
hydrogen; (η-C5H5)NiOs3(CO)9(μ2-H)3 in pentane T=90°C; P=456 Torr; 6 h; var. catalysts, var. conditions; Product distribution;
参考文献
Journal of Organometallic Chemistry, , vol. 241, # 1 p. 99 - 112
反应条件
in 1,2,2-trifluoro-trichloroethane T=100°C; var. temp.; also irradiation; MechanismRate constantProduct distribution;
参考文献
Journal of the American Chemical Society, , vol. 120, # 24 p. 5990 - 5999
反应条件
in chloroform-d1 T=30°C;
参考文献
Chemistry Letters, , # 9 p. 905 - 906