3,3-二甲基-1-丁烯合成路线 （共 347 条）
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=120°C; 6 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., , vol. 126, # 5 p. 1414 - 1418
反应条件
hydrogen; methanesulfonic acid; lt;Pt(C2H4)(DPPB)gt; in toluene T=100°C; P=38000 Torr; var. olefins; Product distribution;
参考文献
Botteghi, Carlo; Paganelli, Stefano
Journal of Organometallic Chemistry, 1991 , vol. 417, # 1/2 p. C41 - C45
反应条件
in 1,2,5-trimethyl-benzene mesitylene, tert-butylethene (Ar); detected by NMR spectra;
参考文献
Kanzelberger; Singh; Czerw; Krogh-Jespersen; Goldman
Journal of the American Chemical Society, 2000 , vol. 122, # 44 p. 11017 - 11018
反应条件
[Ir(6-Neo)(COD)Cl] in ethanol P=3750.38 Torr; 0.5 h;
参考文献
Dunsford, Jay J.; Tromp, Dorette S.; Cavell, Kingsley J.; Elsevier, Cornelis J.; Kariuki, Benson M.
Dalton Transactions, 2013 , vol. 42, # 20 p. 7318 - 7329
反应条件
IrH2{C6H3-2,6-(CH2PBu(t)2)2} in 1,3,5-trimethyl-benzene T=55°C; Kinetics;
参考文献
Renkema, Kenton B.; Kissin, Yury V.; Goldman, Alan S.
Journal of the American Chemical Society, 2003 , vol. 125, # 26 p. 7770 - 7771
反应条件
Mo(=CHCMe2Ph)(N=C6H4iPr2)[OC(Me)(CF3)2]2; 2,6-di(O-PtBu4)C6H3Ir(C2H4) T=125°C; 24 h; Further byproducts.;
参考文献
Ahuja, Ritu; Kundu, Sabuj; Goldman, Alan S.; Brookhart, Maurice; Vicente, Brian C.; Scott, Susannah L.
Chemical Communications, 2008 , # 2 p. 253 - 255
反应条件
{4-O(CH2)3Si(Me)2(OMe)-C6H2-2,6-[OP(t-Bu)2]2}Ir(COE) supported on silica 39 h; Heating; Product distribution / selectivity;
参考文献
Vicente, Brian C.; Huang, Zheng; Brookhart, Maurice; Goldman, Alan S.; Scott, Susannah L.
Dalton Transactions, 2011 , vol. 40, # 16 p. 4268 - 4274
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=120°C; 24 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=120°C; 12 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
C18H32ClIrOP2S; sodium t-butanolate in para-xylene T=120°C; 12 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
