3,3-二甲基-1-丁烯合成路线 (共 347 条)
反应条件
3-methyl-2-amino-pyridine; [RhCl(PPh3)2]; α,α,α-Trifluoro-p-toluic acid in toluene T=110°C; 12 h;
参考文献
Jo, Eun-Ae; Jun, Chul-Ho
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3338 - 3340
反应条件
potassium osmate(VI); diethyl-(2-benzyloxy-ethyl)-amine; 4-methylmorpholine N-oxide in acetone T=20°C; 72 h;
参考文献
Stiasny, Hans Christian
Synthesis, 1996 , # 2 p. 259 - 264
反应条件
in acetic anhydride T=0 - 20°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Loiseau, Andre-Michel; Luft, Robert; Zunino, Serge
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 5-6 p. 144 - 152
反应条件
Yield given. Multistep reaction;
参考文献
Delacre
Chem. Zentralbl., 1906 , vol. 77, # I p. 1233
反应条件
IrH2{C6H3-2,6-(CH2PBu(t)2)2}; Mo(N-2,6-i-Pr2C6H3)(C3H6)(pyr)(2,6-bis(2,4,6-triisopropylphenyl)phenol) T=180°C; Cross Metathesis; 24 h; Schlenk technique;
参考文献
Dobereiner, Graham E.; Yuan, Jian; Schrock, Richard R.; Goldman, Alan S.; Hackenberg, Jason D.
Journal of the American Chemical Society, 2013 , vol. 135, # 34 p. 12572 - 12575
反应条件
in acetonitrile 5 h; Ambient temperatureIrradiation;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 57, # 8 p. 2140 - 2143
反应条件
in tetrachloromethane 1) -20 deg C, 2) up to rt;
参考文献
Tetrahedron, , vol. 37, # 18 p. 3115 - 3120
反应条件
in acetonitrile 4 h; Irradiation;
参考文献
European Journal of Organic Chemistry, , # 17 p. 3229 - 3237
反应条件
IrH2{C6H3-2,6-(CH2PBu(t)2)2}; Mo(N-2,6-i-Pr2C6H3)(C3H6)(pyr)(2,6-bis(2,4,6-triisopropylphenyl)phenol) T=180°C; Cross Metathesis; 24 h; Schlenk technique;
参考文献
Dobereiner, Graham E.; Yuan, Jian; Schrock, Richard R.; Goldman, Alan S.; Hackenberg, Jason D.
Journal of the American Chemical Society, 2013 , vol. 135, # 34 p. 12572 - 12575
参考文献
Doxsee, Kenneth M.; Farahi, Judah B.; Hope, Hakon
Journal of the American Chemical Society, 1991 , vol. 113, # 23 p. 8889 - 8898