3,3-二甲基-1-丁烯合成路线 （共 347 条）
参考文献
Ecke et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 1511
反应条件
C18H32ClIrOP2S; sodium t-butanolate T=100°C; 4 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
C18H32ClIrOP2S; sodium t-butanolate T=200°C; 1 h; Inert atmosphereSchlenk techniqueGloveboxSealed tube; Reagent/catalystConcentrationTime;
参考文献
Yao, Wubing; Zhang, Yuxuan; Jia, Xiangqing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1390 - 1394
Angew. Chem., 2014 , vol. 126, # 5 p. 1414 - 1418
反应条件
[(C6H6)(PCy3)(CO)RuH]+BF4- in chlorobenzene T=110°C; Autoclave;
参考文献
Lee, Dong-Hwan; Kwon, Ki-Hyeok; Yi, Chae S.
Science, 2011 , vol. 333, # 6049 p. 1613 - 1616
参考文献
Jawein
Justus Liebigs Annalen der Chemie, 1879 , vol. 195, p. 255
反应条件
(i) PhSeBr, MeCN, CH2Cl2, (ii) O3, CCl4, (iii) iPr2NH; Multistep reaction;
参考文献
Raucher,S.
Tetrahedron Letters, 1977 , p. 3909 - 3912
反应条件
tri-ruthenium(0)dodecacarbonyl; 2-(dicyclohexylphosphino)-1-methyl-1H-imidazole; water; hydrogen; lithium chloride in 1-methyl-pyrrolidin-2-one T=130°C; P=60 Torr; 20 h; Autoclave; regioselective reaction;
参考文献
Fleischer, Ivana; Dyballa, Katrin Marie; Jennerjahn, Reiko; Jackstell, Ralf; Franke, Robert; Spannenberg, Anke; Beller, Matthias
Angewandte Chemie - International Edition, 2013 , vol. 52, # 10 p. 2949 - 2953
反应条件
lt;RhH(PEt3)3gt;; hydrogen in ethanol T=120°C; P=30400 Torr; 16 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
MacDougall, Joanna K.; Simpson, Michael C.; Green, Michael J.; Cole-Hamilton, David J.
Journal of the Chemical Society - Dalton Transactions, 1996 , # 6 p. 1161 - 1172
反应条件
tri-ruthenium(0)dodecacarbonyl; sodium formate; lithium chloride T=150°C; 24 h; AutoclaveIonic liquid;
参考文献
Mura, Manuel G.; Luca, Lidia De; Giacomelli, Giampaolo; Porcheddu, Andrea
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 17 p. 3180 - 3186
反应条件
hydrogen; cobalt T=120 - 160°C; P=73550.8 - 147102 Torr; Hydrieren des Reaktionproduktes am gleichen Katalysator;
参考文献
Keulemans; Kwantes; van Bavel
Recueil des Travaux Chimiques des Pays-Bas, 1948 , vol. 67, p. 302
